Synthesis of Bis(1,2-dimethylimidazole)copper(I) Hexafluorophosphate: An Experiment Using a Glove Box. Niewahner, H, J, Walters, & A, K. Journal of Chemical Education, 84(4):702, April, 2007.
Synthesis of Bis(1,2-dimethylimidazole)copper(I) Hexafluorophosphate: An Experiment Using a Glove Box [link]Paper  doi  abstract   bibtex   
A lab. expt. suitable for a third-year inorg. chem. lab. is presented that utilizes a glove box. The synthesis of a copper complex that has a distinct color change to indicate byproduct oxidn. by oxygen provides students an opportunity to utilize basic lab. techniques in a glove box to achieve significantly better results than the usage of Schlenk techniques. While a few students had trouble working with the gloves, all have gained an appreciation of the unique challenges and skills needed to utilize this unusual piece of equipment. [on SciFinder (R)]
@article{ Niewahner2007a,
  abstract = {A lab. expt. suitable for a third-year inorg. chem. lab. is presented that utilizes a glove box. The synthesis of a copper complex that has a distinct color change to indicate byproduct oxidn. by oxygen provides students an opportunity to utilize basic lab. techniques in a glove box to achieve significantly better results than the usage of Schlenk techniques. While a few students had trouble working with the gloves, all have gained an appreciation of the unique challenges and skills needed to utilize this unusual piece of equipment. [on SciFinder (R)]},
  annote = {From Duplicate 2 ( },
  author = {Niewahner, J H and Walters, Keith A},
  doi = {10.1021/ed084p702},
  file = {:C$\backslash$:/Users/walterske/SkyDrive/References/Journal of Chemical Education/2007 - Niewahner, Walters - Synthesis of Bis(1,2-dimethylimidazole)copper(I) Hexafluorophosphate An Experiment Using a Glove Box.pdf:pdf},
  isbn = {2132100500},
  issn = {0021-9584},
  journal = {Journal of Chemical Education},
  keywords = {2-dimeth,2-dimethylimidazole)copper (I) hexafluorophosphate,Amines / Ammonium Compounds,Chemical education,Coordination Compounds,Glove boxes,Hands-On Learning / Manipulatives,IR Spectroscopy,Inorganic Chemistry,Laboratory Equipment / Apparatus,Laboratory Instruction,Laboratory experiment (synthesis of bis(1,NMR Spectroscopy,Reactions,Synthesis,Upper-Division Undergraduate,chem education lab copper hexafluorophosphate synt},
  language = {written in English.},
  month = {April},
  number = {4},
  pages = {702},
  title = {{Synthesis of Bis(1,2-dimethylimidazole)copper(I) Hexafluorophosphate: An Experiment Using a Glove Box}},
  url = {http://pubs.acs.org/doi/abs/10.1021/ed084p702},
  volume = {84},
  year = {2007}
}

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