Single-step synthesis of nanostructured γ-alumina with solvent reusability to maximise yield and morphological purity. Bell, T. E., González-Carballo, J. M., Tooze, R. P., & Torrente-Murciano, L. Journal of Materials Chemistry A, 3(11):6196–6201, 2015. ![Single-step synthesis of nanostructured γ-alumina with solvent reusability to maximise yield and morphological purity [link]](https://bibbase.org/img/filetypes/link.svg "link")
Paper doi abstract bibtex The mechanism of the hydrothermal synthesis of nanostructured alumina shows that the NaOH : Al molar ratio affects not only the resulting morphology but also the yield. Successful reusability of the reaction medium opens the door to large scale manufacturing. , Insights of the chemical mechanism for the hydrothermal synthesis of nanostructured alumina are elucidated for the first time, demonstrating the effect of the NaOH : Al molar ratio not only on the resulting morphology of the material but also on the product yield. Highly uniform pure γ-Al 2 O 3 nanorods are synthesised under acidic conditions (pH \textless 4), while basic medium (pH \textgreater 9) lead to γ-Al 2 O 3 nanoplates. Maximisation of the morphological purity leads to a decrease in the overall aluminium yield which can be overcome by successful reusability of the synthesis medium in an effort to increase efficiency (yield and productivity) and minimise waste production towards feasible large-scale manufacturing of nanostructured materials.
@article{bell_single-step_2015,
title = {Single-step synthesis of nanostructured γ-alumina with solvent reusability to maximise yield and morphological purity},
volume = {3},
issn = {2050-7488, 2050-7496},
url = {http://xlink.rsc.org/?DOI=C4TA06692H},
doi = {10.1039/C4TA06692H},
abstract = {The mechanism of the hydrothermal synthesis of nanostructured alumina shows that the NaOH : Al molar ratio affects not only the resulting morphology but also the yield. Successful reusability of the reaction medium opens the door to large scale manufacturing.
,
Insights of the chemical mechanism for the hydrothermal synthesis of nanostructured alumina are elucidated for the first time, demonstrating the effect of the NaOH : Al molar ratio not only on the resulting morphology of the material but also on the product yield. Highly uniform pure γ-Al
2
O
3
nanorods are synthesised under acidic conditions (pH {\textless} 4), while basic medium (pH {\textgreater} 9) lead to γ-Al
2
O
3
nanoplates. Maximisation of the morphological purity leads to a decrease in the overall aluminium yield which can be overcome by successful reusability of the synthesis medium in an effort to increase efficiency (yield and productivity) and minimise waste production towards feasible large-scale manufacturing of nanostructured materials.},
language = {en},
number = {11},
urldate = {2021-02-26},
journal = {Journal of Materials Chemistry A},
author = {Bell, T. E. and González-Carballo, J. M. and Tooze, R. P. and Torrente-Murciano, L.},
year = {2015},
pages = {6196--6201},
}
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