Characterization of an experimental TPD-MS system. Quantitative calibrations. Bernal, S., García, R., & Rodríguez-Izquierdo, J. Thermochimica Acta, 70(1-3):249-256, 1983. cited By 21
Characterization of an experimental TPD-MS system. Quantitative calibrations [link]Paper  doi  abstract   bibtex   
A simple TPD-MS device, which operates in a flow of helium at normal pressure, is described. The system was checked to ensure that it was capable of performing quantitative analysis of evolved gases. Quantitative calibrations were obtained for a number of substances, both organic and inorganic. The influence of several operational variables, which were easily modified in our device, on the response of the system has also been studied. Calibrations were obtained by fast injection into the system of the substances to be analysed. Since these calibrations were obtained in an unusual way, under conditions which are not exactly the same as those operating in real TPD experiments, their applicability to EGA has been tested. © 1983.
@ARTICLE{Bernal1983249,
author={Bernal, S. and García, R. and Rodríguez-Izquierdo, J.M.},
title={Characterization of an experimental TPD-MS system. Quantitative calibrations},
journal={Thermochimica Acta},
year={1983},
volume={70},
number={1-3},
pages={249-256},
doi={10.1016/0040-6031(83)80199-3},
note={cited By 21},
url={https://www.scopus.com/inward/record.url?eid=2-s2.0-0040788534&partnerID=40&md5=fe1cc2361834989975420fd0a960741b},
affiliation={Department of Inorganic Chemistry, Faculty of Sciences, University of Cádiz, Puerto Real, Cádiz, Spain},
abstract={A simple TPD-MS device, which operates in a flow of helium at normal pressure, is described. The system was checked to ensure that it was capable of performing quantitative analysis of evolved gases. Quantitative calibrations were obtained for a number of substances, both organic and inorganic. The influence of several operational variables, which were easily modified in our device, on the response of the system has also been studied. Calibrations were obtained by fast injection into the system of the substances to be analysed. Since these calibrations were obtained in an unusual way, under conditions which are not exactly the same as those operating in real TPD experiments, their applicability to EGA has been tested. © 1983.},
document_type={Article},
source={Scopus},
}

Downloads: 0