Advanced solid state NMR techniques for the characterization of sol-gel-derived materials. Bonhomme, C., Coelho, C., Baccile, N., Gervais, C., Azaïs, T., & Babonneau, F. Accounts of chemical research, 40(9):738–46, September, 2007. ![Advanced solid state NMR techniques for the characterization of sol-gel-derived materials. [link]](https://bibbase.org/img/filetypes/link.svg "link")
Paper doi abstract bibtex A large array of advanced solid state NMR (nuclear magnetic resonance) techniques is presented in the frame of the structural characterization of sol-gel-derived materials. These techniques include the pertinent detection of (17)O chemical shifts, MAS (magic angle spinning) J spectroscopy in the solid state, high-resolution (1)H spectroscopy, heteronuclear and homonuclear D (dipolar)-derived multidimensional correlation experiments, and first-principles calculations of NMR parameters. This spectroscopic approach is suitable for the in-depth description of multicomponent sol-gel derivatives, crystalline and amorphous biocompatible silicophosphates, Al-O-P clusters, and templated porous materials. It offers unique perspectives for the description of the hybrid interfaces in terms of chemical and spatial connectivities.
@article{Bonhomme2007,
title = {Advanced solid state {NMR} techniques for the characterization of sol-gel-derived materials.},
volume = {40},
issn = {0001-4842},
url = {http://www.ncbi.nlm.nih.gov/pubmed/17461543},
doi = {10.1021/ar600030j},
abstract = {A large array of advanced solid state NMR (nuclear magnetic resonance) techniques is presented in the frame of the structural characterization of sol-gel-derived materials. These techniques include the pertinent detection of (17)O chemical shifts, MAS (magic angle spinning) J spectroscopy in the solid state, high-resolution (1)H spectroscopy, heteronuclear and homonuclear D (dipolar)-derived multidimensional correlation experiments, and first-principles calculations of NMR parameters. This spectroscopic approach is suitable for the in-depth description of multicomponent sol-gel derivatives, crystalline and amorphous biocompatible silicophosphates, Al-O-P clusters, and templated porous materials. It offers unique perspectives for the description of the hybrid interfaces in terms of chemical and spatial connectivities.},
number = {9},
journal = {Accounts of chemical research},
author = {Bonhomme, Christian and Coelho, Cristina and Baccile, Niki and Gervais, Christel and Azaïs, Thierry and Babonneau, Florence},
month = sep,
year = {2007},
pmid = {17461543},
pages = {738--46},
}
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