@ARTICLE{Carretero1992203,
author={Carretero, I. and Maldonado, M. and Laserna, J.J. and Bonet, E. and Ramis Ramos, G.},
title={Detection of banned drugs in sport by micellar liquid chromatography},
journal={Analytica Chimica Acta},
year={1992},
volume={259},
number={2},
pages={203-210},
doi={10.1016/0003-2670(92)85369-H},
note={cited By 37},
url={https://www.scopus.com/inward/record.uri?eid=2-s2.0-0026529633&doi=10.1016%2f0003-2670%2892%2985369-H&partnerID=40&md5=e27a48816c3acce8ae3a071feab55944},
affiliation={Department of Analytical Chemistry, Faculty of Sciences, University of Málaga, 29071 Málaga, Spain; Department of Analytical Chemistry, Faculty of Chemistry, University of Valencia, 46100 Burjassot, Spain},
abstract={A rapid method for the determination of banned drugs in sport (including stimulants, anabolic steroids and diuretics) based on micellar liquid chromatography is proposed. The mobile phase is an aqueous solution of a surfactant (sodium dodecyl sulphate in this instance) and the stationary phase is octadecylsilica. The retention parameters of the drugs were established and the effect of a mobile phase organic modifier on the chromatographic behaviour of the compounds was studied. Improvements in efficiency were achieved by control of the temperature of the mobile phase. This method allows the direct injection of urine samples for the determination of drugs excreted free in urine: amiphenazole, amiloride, amphetamine, clostebol, ephedrine, phenylpropanolamine, metandienone, methoxyphenamine, nandrolone and spironolactone. Limits of detection in the nanogram range and relative standard deviations of 1-11% were obtained. © 1992.},
author_keywords={Liquid chromatography;  Micellar chromatography;  Pharmaceuticals;  Urine},
keywords={acetazolamide;  amiloride;  amiphenazole;  amphetamine;  anabolic agent;  bendroflumethiazide;  benzthiazide;  caffeine;  chlortalidone;  clostebol;  diuretic agent;  ephedrine;  etacrynic acid;  furosemide;  hydrochlorothiazide;  meclofenoxate;  metandienone;  methoxyphenamine;  nandrolone;  nikethamide;  pemoline;  phenylpropanolamine;  psychostimulant agent;  spironolactone;  unclassified drug, article;  doping;  drug abuse;  human;  liquid chromatography;  sport;  urinalysis},
chemicals_cas={acetazolamide, 1424-27-7, 59-66-5; amiloride, 2016-88-8, 2609-46-3; amiphenazole, 490-55-1; amphetamine, 1200-47-1, 139-10-6, 156-34-3, 2706-50-5, 300-62-9, 51-62-7, 60-13-9, 60-15-1; bendroflumethiazide, 73-48-3; benzthiazide, 91-33-8; caffeine, 30388-07-9, 58-08-2; chlortalidone, 77-36-1; clostebol, 1093-58-9, 51023-23-5; ephedrine, 299-42-3, 50-98-6; etacrynic acid, 58-54-8; furosemide, 54-31-9; hydrochlorothiazide, 58-93-5; meclofenoxate, 3685-84-5, 51-68-3; metandienone, 72-63-9; methoxyphenamine, 5588-10-3, 93-30-1; nandrolone, 434-22-0; nikethamide, 59-26-7; pemoline, 2152-34-3; phenylpropanolamine, 14838-15-4, 154-41-6, 4345-16-8, 48115-38-4; spironolactone, 52-01-7},
references={Voy, (1988) Encyclopaedia of Sports Medicine, 1. , A. Dirix, H.G. Knuttgen, K. Tittel, Sports Medicine, International Olympic Committee, Blackwell, Oxford; Catlin, Kammerer, Hatton, Sekera, Merdink, (1987) Clin. Chem., 33, p. 319; (1988) Int. Labmate, 13, p. 39; Berthod, Dorsey, (1988) Analusis, 16, p. 75; Armstrong, (1985) Sep. Purif. Methods, 14, p. 213; Berthod, Asensio, Laserna, (1989) J. Liq. Chromatogr., 12, p. 2621; Fraga, González, Sanz-Medel, Determination of some anticancer 6-thiopurine compounds by high-performance liquid chromatography with micelles as the mobile phase (1988) Analytica Chimica Acta, 212, p. 181; Arunyanart, Cline Love, (1985) J. Chromatogr., 342, p. 293; Armstrong, Henry, (1980) J. Liq. Chromatogr., 3, p. 657; Dorsey, (1987) Adv. Chromatogr., 27, p. 167; Dorsey, de Echegaray, Landy, (1983) Anal. Chem., 55, p. 924; Foley, Dorsey, (1983) Anal. Chem., 55, p. 730; Tomasella, Fett, Cline Love, (1991) Anal. Chem., 63, p. 474; Khaledi, Peuler, Ngeh-Ngwainbi, (1987) Anal. Chem., 59, p. 2738; Khaledi, (1988) Anal. Chem., 60, p. 876; Donike, (1988) Encylopaedia of Sports Medicine, 1. , A. Dirix, H.G. Knuttgen, K. Tittel, Sports Medicine, International Olympic Committee, Blackwell, Oxford},
correspondence_address1={Carretero, I.; Department of Analytical Chemistry, Faculty of Sciences, University of Málaga, 29071 Málaga, Spain},
issn={00032670},
coden={ACACA},
language={English},
abbrev_source_title={Anal. Chim. Acta},
document_type={Article},
source={Scopus},
}

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The mobile phase is an aqueous solution of a surfactant (sodium dodecyl sulphate in this instance) and the stationary phase is octadecylsilica. The retention parameters of the drugs were established and the effect of a mobile phase organic modifier on the chromatographic behaviour of the compounds was studied. Improvements in efficiency were achieved by control of the temperature of the mobile phase. This method allows the direct injection of urine samples for the determination of drugs excreted free in urine: amiphenazole, amiloride, amphetamine, clostebol, ephedrine, phenylpropanolamine, metandienone, methoxyphenamine, nandrolone and spironolactone. Limits of detection in the nanogram range and relative standard deviations of 1-11% were obtained. © 1992.","author_keywords":"Liquid chromatography; Micellar chromatography; Pharmaceuticals; Urine","keywords":"acetazolamide; amiloride; amiphenazole; amphetamine; anabolic agent; bendroflumethiazide; benzthiazide; caffeine; chlortalidone; clostebol; diuretic agent; ephedrine; etacrynic acid; furosemide; hydrochlorothiazide; meclofenoxate; metandienone; methoxyphenamine; nandrolone; nikethamide; pemoline; phenylpropanolamine; psychostimulant agent; spironolactone; unclassified drug, article; doping; drug abuse; human; liquid chromatography; sport; urinalysis","chemicals_cas":"acetazolamide, 1424-27-7, 59-66-5; amiloride, 2016-88-8, 2609-46-3; amiphenazole, 490-55-1; amphetamine, 1200-47-1, 139-10-6, 156-34-3, 2706-50-5, 300-62-9, 51-62-7, 60-13-9, 60-15-1; bendroflumethiazide, 73-48-3; benzthiazide, 91-33-8; caffeine, 30388-07-9, 58-08-2; chlortalidone, 77-36-1; clostebol, 1093-58-9, 51023-23-5; ephedrine, 299-42-3, 50-98-6; etacrynic acid, 58-54-8; furosemide, 54-31-9; hydrochlorothiazide, 58-93-5; meclofenoxate, 3685-84-5, 51-68-3; metandienone, 72-63-9; methoxyphenamine, 5588-10-3, 93-30-1; nandrolone, 434-22-0; nikethamide, 59-26-7; pemoline, 2152-34-3; phenylpropanolamine, 14838-15-4, 154-41-6, 4345-16-8, 48115-38-4; spironolactone, 52-01-7","references":"Voy, (1988) Encyclopaedia of Sports Medicine, 1. , A. 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Chem., 60, p. 876; Donike, (1988) Encylopaedia of Sports Medicine, 1. , A. Dirix, H.G. Knuttgen, K. Tittel, Sports Medicine, International Olympic Committee, Blackwell, Oxford","correspondence_address1":"Carretero, I.; Department of Analytical Chemistry, Faculty of Sciences, University of Málaga, 29071 Málaga, Spain","issn":"00032670","coden":"ACACA","language":"English","abbrev_source_title":"Anal. Chim. Acta","document_type":"Article","source":"Scopus","bibtex":"@ARTICLE{Carretero1992203,\nauthor={Carretero, I. and Maldonado, M. and Laserna, J.J. and Bonet, E. and Ramis Ramos, G.},\ntitle={Detection of banned drugs in sport by micellar liquid chromatography},\njournal={Analytica Chimica Acta},\nyear={1992},\nvolume={259},\nnumber={2},\npages={203-210},\ndoi={10.1016/0003-2670(92)85369-H},\nnote={cited By 37},\nurl={https://www.scopus.com/inward/record.uri?eid=2-s2.0-0026529633&doi=10.1016%2f0003-2670%2892%2985369-H&partnerID=40&md5=e27a48816c3acce8ae3a071feab55944},\naffiliation={Department of Analytical Chemistry, Faculty of Sciences, University of Málaga, 29071 Málaga, Spain; Department of Analytical Chemistry, Faculty of Chemistry, University of Valencia, 46100 Burjassot, Spain},\nabstract={A rapid method for the determination of banned drugs in sport (including stimulants, anabolic steroids and diuretics) based on micellar liquid chromatography is proposed. The mobile phase is an aqueous solution of a surfactant (sodium dodecyl sulphate in this instance) and the stationary phase is octadecylsilica. The retention parameters of the drugs were established and the effect of a mobile phase organic modifier on the chromatographic behaviour of the compounds was studied. Improvements in efficiency were achieved by control of the temperature of the mobile phase. This method allows the direct injection of urine samples for the determination of drugs excreted free in urine: amiphenazole, amiloride, amphetamine, clostebol, ephedrine, phenylpropanolamine, metandienone, methoxyphenamine, nandrolone and spironolactone. Limits of detection in the nanogram range and relative standard deviations of 1-11% were obtained. © 1992.},\nauthor_keywords={Liquid chromatography; Micellar chromatography; Pharmaceuticals; Urine},\nkeywords={acetazolamide; amiloride; amiphenazole; amphetamine; anabolic agent; bendroflumethiazide; benzthiazide; caffeine; chlortalidone; clostebol; diuretic agent; ephedrine; etacrynic acid; furosemide; hydrochlorothiazide; meclofenoxate; metandienone; methoxyphenamine; nandrolone; nikethamide; pemoline; phenylpropanolamine; psychostimulant agent; spironolactone; unclassified drug, article; doping; drug abuse; human; liquid chromatography; sport; urinalysis},\nchemicals_cas={acetazolamide, 1424-27-7, 59-66-5; amiloride, 2016-88-8, 2609-46-3; amiphenazole, 490-55-1; amphetamine, 1200-47-1, 139-10-6, 156-34-3, 2706-50-5, 300-62-9, 51-62-7, 60-13-9, 60-15-1; bendroflumethiazide, 73-48-3; benzthiazide, 91-33-8; caffeine, 30388-07-9, 58-08-2; chlortalidone, 77-36-1; clostebol, 1093-58-9, 51023-23-5; ephedrine, 299-42-3, 50-98-6; etacrynic acid, 58-54-8; furosemide, 54-31-9; hydrochlorothiazide, 58-93-5; meclofenoxate, 3685-84-5, 51-68-3; metandienone, 72-63-9; methoxyphenamine, 5588-10-3, 93-30-1; nandrolone, 434-22-0; nikethamide, 59-26-7; pemoline, 2152-34-3; phenylpropanolamine, 14838-15-4, 154-41-6, 4345-16-8, 48115-38-4; spironolactone, 52-01-7},\nreferences={Voy, (1988) Encyclopaedia of Sports Medicine, 1. , A. Dirix, H.G. Knuttgen, K. Tittel, Sports Medicine, International Olympic Committee, Blackwell, Oxford; Catlin, Kammerer, Hatton, Sekera, Merdink, (1987) Clin. Chem., 33, p. 319; (1988) Int. Labmate, 13, p. 39; Berthod, Dorsey, (1988) Analusis, 16, p. 75; Armstrong, (1985) Sep. Purif. Methods, 14, p. 213; Berthod, Asensio, Laserna, (1989) J. Liq. Chromatogr., 12, p. 2621; Fraga, González, Sanz-Medel, Determination of some anticancer 6-thiopurine compounds by high-performance liquid chromatography with micelles as the mobile phase (1988) Analytica Chimica Acta, 212, p. 181; Arunyanart, Cline Love, (1985) J. Chromatogr., 342, p. 293; Armstrong, Henry, (1980) J. Liq. Chromatogr., 3, p. 657; Dorsey, (1987) Adv. Chromatogr., 27, p. 167; Dorsey, de Echegaray, Landy, (1983) Anal. Chem., 55, p. 924; Foley, Dorsey, (1983) Anal. Chem., 55, p. 730; Tomasella, Fett, Cline Love, (1991) Anal. Chem., 63, p. 474; Khaledi, Peuler, Ngeh-Ngwainbi, (1987) Anal. Chem., 59, p. 2738; Khaledi, (1988) Anal. Chem., 60, p. 876; Donike, (1988) Encylopaedia of Sports Medicine, 1. , A. Dirix, H.G. Knuttgen, K. Tittel, Sports Medicine, International Olympic Committee, Blackwell, Oxford},\ncorrespondence_address1={Carretero, I.; Department of Analytical Chemistry, Faculty of Sciences, University of Málaga, 29071 Málaga, Spain},\nissn={00032670},\ncoden={ACACA},\nlanguage={English},\nabbrev_source_title={Anal. Chim. 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