A hydration study by XRD/Rietveld analysis of cement regenerated from completely recyclable concrete. De Schepper, M., De Buysser, K., Van Driessche, I., & De Belie, N. In NTCC2014 : international conference on non-traditional cement and concrete, Brno, Czech Republic, 2014. Novpress.
Paper abstract bibtex In today’s cement and concrete research, mineralogical quantification of (un)hydrated cement samples by X-ray Diffraction/Rietveld analysis becomes more and more important. As the results from XRD/Rietveld analysis are becoming increasingly more accurate, it became a widely used tool to study the hydration of cementitious materials besides other techniques e.g. isothermal calorimetry or thermogravimetric analysis. To quantify amorphous or non-identified phases, an internal standard might be added to estimate these so-called ‘other’ phases. Compared to unhydrated samples which are almost completely crystalline, it has a higher significance in hydrated samples, as certain cement hydrates, such as C-S-H, hydrogarnet, hydrotalcite, AFm, etc., are often poorly crystalline. Within the development of Completely Recyclable Concrete (CRC – a concrete designed for reincarnation within the cement production following the Cradle-to-Cradle Principle) the hydration of the regenerated cement was assessed by XRD/Rietveld analysis. Within this study it was found that the particle size distributions of the sample and the internal standard should not be underestimated within the quantification of the ‘other’ phases.
@inproceedings{de_schepper_hydration_2014,
address = {Brno, Czech Republic},
title = {A hydration study by {XRD}/{Rietveld} analysis of cement regenerated from completely recyclable concrete},
copyright = {I have transferred the copyright for this publication to the publisher},
isbn = {978-80-214-4867-4},
url = {http://hdl.handle.net/1854/LU-5743848},
abstract = {In today’s cement and concrete research, mineralogical quantification of (un)hydrated cement samples by X-ray Diffraction/Rietveld analysis becomes more and more important. As the results from XRD/Rietveld analysis are becoming increasingly more accurate, it became a widely used tool to study the hydration of cementitious materials besides other techniques e.g. isothermal calorimetry or thermogravimetric analysis. To quantify amorphous or non-identified phases, an internal standard might be added to estimate these so-called ‘other’ phases. Compared to unhydrated samples which are almost completely crystalline, it has a higher significance in hydrated samples, as certain cement hydrates, such as C-S-H, hydrogarnet, hydrotalcite, AFm, etc., are often poorly crystalline. Within the development of Completely Recyclable Concrete (CRC – a concrete designed for reincarnation within the cement production following the Cradle-to-Cradle Principle) the hydration of the regenerated cement was assessed by XRD/Rietveld analysis. Within this study it was found that the particle size distributions of the sample and the internal standard should not be underestimated within the quantification of the ‘other’ phases.},
language = {en},
urldate = {2018-03-29},
booktitle = {{NTCC}2014 : international conference on non-traditional cement and concrete},
publisher = {Novpress},
author = {De Schepper, Mieke and De Buysser, Klaartje and Van Driessche, Isabel and De Belie, Nele},
year = {2014}
}
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As the results from XRD/Rietveld analysis are becoming increasingly more accurate, it became a widely used tool to study the hydration of cementitious materials besides other techniques e.g. isothermal calorimetry or thermogravimetric analysis. To quantify amorphous or non-identified phases, an internal standard might be added to estimate these so-called ‘other’ phases. Compared to unhydrated samples which are almost completely crystalline, it has a higher significance in hydrated samples, as certain cement hydrates, such as C-S-H, hydrogarnet, hydrotalcite, AFm, etc., are often poorly crystalline. Within the development of Completely Recyclable Concrete (CRC – a concrete designed for reincarnation within the cement production following the Cradle-to-Cradle Principle) the hydration of the regenerated cement was assessed by XRD/Rietveld analysis. 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