Carbon nanotube-modified monolithic polymethacrylate pipette tips for (micro)solid-phase extraction of antidepressants from urine samples

Carbon nanotube-modified monolithic polymethacrylate pipette tips for (micro)solid-phase extraction of antidepressants from urine samples. Fresco-Cala, B., Mompó-Roselló, Ó., Simó-Alfonso, E., Cárdenas, S., & Herrero-Martínez, J. Microchimica Acta, Springer-Verlag Wien, 2018. cited By 48

Paper doi abstract bibtex

This work evaluates the potential of methacrylate monoliths with multi-walled carbon nanotubes incorporated into the polymeric network for the extraction of antidepressants from human urine. The method is based on a micropipette solid-phase extraction tip containing a hybrid monolithic material covalently attached to the polypropylene housing. A polymer layer made from poly(ethylene dimethacrylate) was bound to the inner surface of a polypropylene tip via UV grafting. The preparation of the monolith and the microextraction steps were optimized in terms of adsorption capacity. Limits of detection ranged from 9 to 15 μg·L−1. The average precision of the method varied between 3 and 5% (intra-tips), and from 4 to 14% (inter-tips). The accuracy of the method was evaluated through a recovery study by using spiked samples. [Figure not available: see fulltext.]. © 2018, Springer-Verlag GmbH Austria, part of Springer Nature.

@ARTICLE{Fresco-Cala2018,
author={Fresco-Cala, B. and Mompó-Roselló, Ó. and Simó-Alfonso, E.F. and Cárdenas, S. and Herrero-Martínez, J.M.},
title={Carbon nanotube-modified monolithic polymethacrylate pipette tips for (micro)solid-phase extraction of antidepressants from urine samples},
journal={Microchimica Acta},
year={2018},
volume={185},
number={2},
doi={10.1007/s00604-017-2659-4},
art_number={127},
note={cited By 48},
url={https://www.scopus.com/inward/record.uri?eid=2-s2.0-85040985542&doi=10.1007%2fs00604-017-2659-4&partnerID=40&md5=d3f06ff857e4e4593cea694215f8fbb2},
affiliation={Departamento de Química Analítica, Instituto Universitario de Investigación en Química Fina y Nanoquímica IUNAN, Universidad de Córdoba, Campus de Rabanales, Edificio Marie Curie, Córdoba, E-14071, Spain; Department of Analytical Chemistry, University of Valencia, Dr. Moliner 50, Burjassot, Valencia  46100, Spain},
abstract={This work evaluates the potential of methacrylate monoliths with multi-walled carbon nanotubes incorporated into the polymeric network for the extraction of antidepressants from human urine. The method is based on a micropipette solid-phase extraction tip containing a hybrid monolithic material covalently attached to the polypropylene housing. A polymer layer made from poly(ethylene dimethacrylate) was bound to the inner surface of a polypropylene tip via UV grafting. The preparation of the monolith and the microextraction steps were optimized in terms of adsorption capacity. Limits of detection ranged from 9 to 15 μg·L−1. The average precision of the method varied between 3 and 5% (intra-tips), and from 4 to 14% (inter-tips). The accuracy of the method was evaluated through a recovery study by using spiked samples. [Figure not available: see fulltext.]. © 2018, Springer-Verlag GmbH Austria, part of Springer Nature.},
author_keywords={Biological samples;  Carbon nanoparticles;  Drugs;  Hybrid monolith;  Liquid chromatography;  Microextraction;  Photografting process;  Porous polymer;  UV attachment},
keywords={antidepressant agent;  carbon nanotube;  polymethacrylic acid;  polymethacrylic acid derivative, adsorption;  chemistry;  equipment design;  human;  isolation and purification;  limit of detection;  procedures;  solid phase microextraction;  urine, Adsorption;  Antidepressive Agents;  Equipment Design;  Humans;  Limit of Detection;  Nanotubes, Carbon;  Polymethacrylic Acids;  Solid Phase Microextraction},
chemicals_cas={polymethacrylic acid, 25087-26-7; Antidepressive Agents; Nanotubes, Carbon; polymethacrylic acid; Polymethacrylic Acids},
references={Bridge, J.A., Iyengar, S., Salary, C.B., Barbe, R.P., Birmaher, B., Pincus, H.A., Ren, L., Brent, D.A., Clinical response and risk for reported suicidal ideation and suicide attempts in pediatric antidepressant treatment: a meta-analysis of randomized controlled trials (2007) JAMA, 297 (15), pp. 1683-1696. , COI: 1:CAS:528:DC%2BD2sXksVChsL4%3D; Ruiz-Angel, M., Carda-Broch, S., Simó-Alfonso, E., Garcí, M., Optimised procedures for the reversed-phase liquid chromatographic analysis of formulations containing tricyclic antidepressants (2003) J Pharm Biomed Anal, 32 (1), pp. 71-84. , COI: 1:CAS:528:DC%2BD3sXivFGjsro%3D; Reuben, B.G., Wittcoff, H.A., Pharmaceutical Chemicals in Perspective (1990) Int Clin Psychopharmacol, 5 (4), p. 299; Alves, C., Fernandes, C., José dos Santos Neto, A., Rodrigues, J.C., Costa Queiroz, M.E., Lanças, F.M., Optimization of the SPME parameters and its online coupling with HPLC for the analysis of tricyclic antidepressants in plasma samples (2006) J Chromatogr Sci, 44 (6), pp. 340-346. , COI: 1:CAS:528:DC%2BD28XmvVCqsLk%3D; Tanaka, E., Terada, M., Nakamura, T., Misawa, S., Wakasugi, C., Forensic analysis of eleven cyclic antidepressants in human biological samples using a new reversed-phase chromatographic column of 2 μm porous microspherical silica gel (1997) J Chromatogr B Biomed Appl, 692 (2), pp. 405-412. , COI: 1:CAS:528:DyaK2sXisFKls70%3D; Uddin, M.N., Samanidou, V.F., Papadoyannis, I.N., Development and validation of an HPLC method for the determination of benzodiazepines and tricyclic antidepressants in biological fluids after sequential SPE (2008) J Sep Sci, 31 (13), pp. 2358-2370. , COI: 1:CAS:528:DC%2BD1cXpsFOht70%3D; Saito, Y., Kawazoe, M., Hayashida, M., Jinno, K., Direct coupling of microcolumn liquid chromatography with in-tube solid-phase microextraction for the analysis of antidepressant drugs (2000) Analyst, 125 (5), pp. 807-809. , COI: 1:CAS:528:DC%2BD3cXivFemtrY%3D; Ghambarian, M., Yamini, Y., Esrafili, A., Three-phase hollow fiber microextraction based on two immiscible organic solvents for determination of tricyclic antidepressant drugs: comparison with conventional three-phase hollow fiber microextraction (2012) J Chromatogr A, 1222, pp. 5-12. , COI: 1:CAS:528:DC%2BC38XovFOrsw%3D%3D; Ito, R., Ushiro, M., Takahashi, Y., Saito, K., Ookubo, T., Iwasaki, Y., Nakazawa, H., Improvement and validation the method using dispersive liquid–liquid microextraction with in situ derivatization followed by gas chromatography–mass spectrometry for determination of tricyclic antidepressants in human urine samples (2011) J Chromatogr B, 879 (31), pp. 3714-3720. , COI: 1:CAS:528:DC%2BC3MXhsFSktrvK; Jiménez-Soto, J.M., Cárdenas, S., Valcárcel, M., Evaluation of carbon nanocones/disks as sorbent material for solid-phase extraction (2009) J Chromatogr A, 1216 (30), pp. 5626-5633; Jiménez-Soto, J.M., Lucena, R., Cárdenas, S., Valcárcel, M., Solid phase (micro)extraction tools based on carbon nanotubes and related nanostructures (2010) Carbon Nanotubes, , https://doi.org/10.5772/39437, InTech, In:, Marulanda, JM, (ed); Pyrzynska, K., Carbon nanotubes as sorbents in the analysis of pesticides (2011) Chemosphere, 83 (11), pp. 1407-1413. , COI: 1:CAS:528:DC%2BC3MXmtFyltrg%3D; Chen, W., Duan, L., Zhu, D., Adsorption of polar and nonpolar organic chemicals to carbon nanotubes (2007) Environ Sci Technol, 41 (24), pp. 8295-8300. , COI: 1:CAS:528:DC%2BD2sXhtlWqsL3I; Valcarcel, M., Simonet, B.M., Cardenas, S., Suárez, B., Present and future applications of carbon nanotubes to analytical science (2005) Anal Bioanal Chem, 382 (8), pp. 1783-1790. , COI: 1:CAS:528:DC%2BD2MXpt1ahsbc%3D; Roldán-Pijuán, M., Lucena, R., Cárdenas, S., Valcárcel, M., Micro-solid phase extraction based on oxidized single-walled carbon nanohorns immobilized on a stir borosilicate disk: application to the preconcentration of the endocrine disruptor benzophenone-3 (2014) Microchem J, 115, pp. 87-94; Es’haghi, Z., Ebrahimi, M., Hosseini, M.-S., Optimization of a novel method for determination of benzene, toluene, ethylbenzene, and xylenes in hair and waste water samples by carbon nanotubes reinforced sol–gel based hollow fiber solid phase microextraction and gas chromatography using factorial experimental design (2011) J Chromatogr A, 1218 (21), pp. 3400-3406; Fresco-Cala, B., Cárdenas, S., Valcárcel, M., Improved microextraction of selected triazines using polymer monoliths modified with carboxylated multi-walled carbon nanotubes (2016) Microchim Acta, 183 (1), pp. 465-474. , COI: 1:CAS:528:DC%2BC2MXhvVSltb7F; Wang, X., Li, X., Li, Z., Zhang, Y., Bai, Y., Liu, H., Online coupling of in-tube solid-phase microextraction with direct analysis in real time mass spectrometry for rapid determination of triazine herbicides in water using carbon-nanotubes-incorporated polymer monolith (2014) Anal Chem, 86 (10), pp. 4739-4747. , COI: 1:CAS:528:DC%2BC2cXmsVGlt7o%3D; Fresco-Cala, B., Cárdenas, S., Valcárcel, M., Preparation and evaluation of micro and meso porous silica monoliths with embedded carbon nanoparticles for the extraction of non-polar compounds from waters (2016) J Chromatogr A, 1468, pp. 55-63. , COI: 1:CAS:528:DC%2BC28XhsFOrtr7E; Lucena, R., Cárdenas, S., Ramis-ramos, G., Valcárcel, M., Herrero-martínez, J.M., UV-polymerized butyl methacrylate monoliths with embedded carboxylic single-walled carbon nanotubes for CEC applications (2014) Anal Bioanal Chem, 406 (25), p. 6329; Fresco-Cala, B., Cárdenas, S., Herrero-Martínez, J.M., Preparation of porous methacrylate monoliths with oxidized single-walled carbon nanohorns for the extraction of nonsteroidal anti-inflammatory drugs from urine samples (2017) Microchim Acta, 184 (6), pp. 1863-1871. , COI: 1:CAS:528:DC%2BC2sXltlKrsb8%3D; Alwael, H., Connolly, D., Clarke, P., Thompson, R., Twamley, B., O'Connor, B., Paull, B., Pipette-tip selective extraction of glycoproteins with lectin modified gold nano-particles on a polymer monolithic phase (2011) Analyst, 136 (12), pp. 2619-2628. , COI: 1:CAS:528:DC%2BC3MXmslOqtL8%3D; Stachowiak, T.B., Rohr, T., Hilder, E.F., Peterson, D.S., Yi, M., Svec, F., Frechet, J.M., Fabrication of porous polymer monoliths covalently attached to the walls of channels in plastic microdevices (2003) Electrophoresis, 24 (21), pp. 3689-3693. , COI: 1:CAS:528:DC%2BD3sXpsFGjsb0%3D; Krenkova, J., Foret, F., Nanoparticle-modified monolithic pipette tips for phosphopeptide enrichment (2013) Anal Bioanal Chem, 405 (7), pp. 1-9; Ma, H., Davis, R.H., Bowman, C.N., A novel sequential photoinduced living graft polymerization (2000) Macromolecules, 33 (2), pp. 331-335. , COI: 1:CAS:528:DyaK1MXotFKgtbc%3D; Rajabi, A.A., Yamini, Y., Faraji, M., Seidi, S., Solid-phase microextraction based on cetyltrimethylammonium bromide-coated magnetic nanoparticles for determination of antidepressants from biological fluids (2013) Med Chem Res, 22 (4), pp. 1570-1577. , COI: 1:CAS:528:DC%2BC38XptFCktb8%3D; Banitaba, M.H., Davarani, S.S.H., Ahmar, H., Movahed, S.K., Application of a new fiber coating based on electrochemically reduced graphene oxide for the cold-fiber headspace solid-phase microextraction of tricyclic antidepressants (2014) J Sep Sci, 37 (9-10), pp. 1162-1169. , COI: 1:CAS:528:DC%2BC2cXmsVKrsbk%3D; Jafari, M., Sedghi, R., Ebrahimzadeh, H., A platinum wire coated with a composite consisting of poly pyrrole and poly (ɛ-caprolactone) for solid phase microextraction of the antidepressant imipramine prior to its determination via ion mobility spectrometry (2016) Microchim Acta, 183 (2), pp. 805-812. , COI: 1:CAS:528:DC%2BC2MXitFSltr%2FL; Alidoust, M., Seidi, S., Rouhollahi, A., Shanehsaz, M., In-tube electrochemically controlled solid phase microextraction of amitriptyline, imipramine and chlorpromazine from human plasma by using an indole-thiophene copolymer nanocomposite (2017) Microchim Acta, 184 (7), pp. 2473-2481. , COI: 1:CAS:528:DC%2BC2sXmvVCltrg%3D; Bagheri, H., Banihashemi, S., Zandian, F.K., Microextraction of antidepressant drugs into syringes packed with a nanocomposite consisting of polydopamine, silver nanoparticles and polypyrrole (2016) Microchim Acta, 183 (1), pp. 195-202. , COI: 1:CAS:528:DC%2BC2MXhsVequrfE; Ata, Ş., Berber, M., Çabuk, H., Akyüz, M., Optimization of magnetic extraction by experimental design methodology for the determination of antidepressants in biological samples (2015) Anal Methods, 7 (15), pp. 6231-6242. , COI: 1:CAS:528:DC%2BC2MXhtVyhtbrP; Kamaruzaman, S., Sanagi, M.M., Yahaya, N., Wan Ibrahim, W.A., Endud, S., Ibrahim, W., Nazihah, W., Magnetic micro-solid-phase extraction based on magnetite-MCM-41 with gas chromatography–mass spectrometry for the determination of antidepressant drugs in biological fluids (2017) J Sep Sci, 40 (21), pp. 4222-4233. , COI: 1:CAS:528:DC%2BC2sXhslygsrjK},
correspondence_address1={Cárdenas, S.; Departamento de Química Analítica, Campus de Rabanales, Edificio Marie Curie, Spain; email: scardenas@uco.es},
publisher={Springer-Verlag Wien},
issn={00263672},
coden={MIACA},
pubmed_id={29594510},
language={English},
abbrev_source_title={Microchim. Acta},
document_type={Article},
source={Scopus},
}

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The method is based on a micropipette solid-phase extraction tip containing a hybrid monolithic material covalently attached to the polypropylene housing. A polymer layer made from poly(ethylene dimethacrylate) was bound to the inner surface of a polypropylene tip via UV grafting. The preparation of the monolith and the microextraction steps were optimized in terms of adsorption capacity. Limits of detection ranged from 9 to 15 μg·L−1. The average precision of the method varied between 3 and 5% (intra-tips), and from 4 to 14% (inter-tips). The accuracy of the method was evaluated through a recovery study by using spiked samples. [Figure not available: see fulltext.]. © 2018, Springer-Verlag GmbH Austria, part of Springer Nature.","author_keywords":"Biological samples; Carbon nanoparticles; Drugs; Hybrid monolith; Liquid chromatography; Microextraction; Photografting process; Porous polymer; UV attachment","keywords":"antidepressant agent; carbon nanotube; polymethacrylic acid; polymethacrylic acid derivative, adsorption; chemistry; equipment design; human; isolation and purification; limit of detection; procedures; solid phase microextraction; urine, Adsorption; Antidepressive Agents; Equipment Design; Humans; Limit of Detection; Nanotubes, Carbon; Polymethacrylic Acids; Solid Phase Microextraction","chemicals_cas":"polymethacrylic acid, 25087-26-7; Antidepressive Agents; Nanotubes, Carbon; polymethacrylic acid; Polymethacrylic Acids","references":"Bridge, J.A., Iyengar, S., Salary, C.B., Barbe, R.P., Birmaher, B., Pincus, H.A., Ren, L., Brent, D.A., Clinical response and risk for reported suicidal ideation and suicide attempts in pediatric antidepressant treatment: a meta-analysis of randomized controlled trials (2007) JAMA, 297 (15), pp. 1683-1696. , COI: 1:CAS:528:DC%2BD2sXksVChsL4%3D; Ruiz-Angel, M., Carda-Broch, S., Simó-Alfonso, E., Garcí, M., Optimised procedures for the reversed-phase liquid chromatographic analysis of formulations containing tricyclic antidepressants (2003) J Pharm Biomed Anal, 32 (1), pp. 71-84. , COI: 1:CAS:528:DC%2BD3sXivFGjsro%3D; Reuben, B.G., Wittcoff, H.A., Pharmaceutical Chemicals in Perspective (1990) Int Clin Psychopharmacol, 5 (4), p. 299; Alves, C., Fernandes, C., José dos Santos Neto, A., Rodrigues, J.C., Costa Queiroz, M.E., Lanças, F.M., Optimization of the SPME parameters and its online coupling with HPLC for the analysis of tricyclic antidepressants in plasma samples (2006) J Chromatogr Sci, 44 (6), pp. 340-346. , COI: 1:CAS:528:DC%2BD28XmvVCqsLk%3D; Tanaka, E., Terada, M., Nakamura, T., Misawa, S., Wakasugi, C., Forensic analysis of eleven cyclic antidepressants in human biological samples using a new reversed-phase chromatographic column of 2 μm porous microspherical silica gel (1997) J Chromatogr B Biomed Appl, 692 (2), pp. 405-412. , COI: 1:CAS:528:DyaK2sXisFKls70%3D; Uddin, M.N., Samanidou, V.F., Papadoyannis, I.N., Development and validation of an HPLC method for the determination of benzodiazepines and tricyclic antidepressants in biological fluids after sequential SPE (2008) J Sep Sci, 31 (13), pp. 2358-2370. , COI: 1:CAS:528:DC%2BD1cXpsFOht70%3D; Saito, Y., Kawazoe, M., Hayashida, M., Jinno, K., Direct coupling of microcolumn liquid chromatography with in-tube solid-phase microextraction for the analysis of antidepressant drugs (2000) Analyst, 125 (5), pp. 807-809. , COI: 1:CAS:528:DC%2BD3cXivFemtrY%3D; Ghambarian, M., Yamini, Y., Esrafili, A., Three-phase hollow fiber microextraction based on two immiscible organic solvents for determination of tricyclic antidepressant drugs: comparison with conventional three-phase hollow fiber microextraction (2012) J Chromatogr A, 1222, pp. 5-12. , COI: 1:CAS:528:DC%2BC38XovFOrsw%3D%3D; Ito, R., Ushiro, M., Takahashi, Y., Saito, K., Ookubo, T., Iwasaki, Y., Nakazawa, H., Improvement and validation the method using dispersive liquid–liquid microextraction with in situ derivatization followed by gas chromatography–mass spectrometry for determination of tricyclic antidepressants in human urine samples (2011) J Chromatogr B, 879 (31), pp. 3714-3720. , COI: 1:CAS:528:DC%2BC3MXhsFSktrvK; Jiménez-Soto, J.M., Cárdenas, S., Valcárcel, M., Evaluation of carbon nanocones/disks as sorbent material for solid-phase extraction (2009) J Chromatogr A, 1216 (30), pp. 5626-5633; Jiménez-Soto, J.M., Lucena, R., Cárdenas, S., Valcárcel, M., Solid phase (micro)extraction tools based on carbon nanotubes and related nanostructures (2010) Carbon Nanotubes, , https://doi.org/10.5772/39437, InTech, In:, Marulanda, JM, (ed); Pyrzynska, K., Carbon nanotubes as sorbents in the analysis of pesticides (2011) Chemosphere, 83 (11), pp. 1407-1413. , COI: 1:CAS:528:DC%2BC3MXmtFyltrg%3D; Chen, W., Duan, L., Zhu, D., Adsorption of polar and nonpolar organic chemicals to carbon nanotubes (2007) Environ Sci Technol, 41 (24), pp. 8295-8300. , COI: 1:CAS:528:DC%2BD2sXhtlWqsL3I; Valcarcel, M., Simonet, B.M., Cardenas, S., Suárez, B., Present and future applications of carbon nanotubes to analytical science (2005) Anal Bioanal Chem, 382 (8), pp. 1783-1790. , COI: 1:CAS:528:DC%2BD2MXpt1ahsbc%3D; Roldán-Pijuán, M., Lucena, R., Cárdenas, S., Valcárcel, M., Micro-solid phase extraction based on oxidized single-walled carbon nanohorns immobilized on a stir borosilicate disk: application to the preconcentration of the endocrine disruptor benzophenone-3 (2014) Microchem J, 115, pp. 87-94; Es’haghi, Z., Ebrahimi, M., Hosseini, M.-S., Optimization of a novel method for determination of benzene, toluene, ethylbenzene, and xylenes in hair and waste water samples by carbon nanotubes reinforced sol–gel based hollow fiber solid phase microextraction and gas chromatography using factorial experimental design (2011) J Chromatogr A, 1218 (21), pp. 3400-3406; Fresco-Cala, B., Cárdenas, S., Valcárcel, M., Improved microextraction of selected triazines using polymer monoliths modified with carboxylated multi-walled carbon nanotubes (2016) Microchim Acta, 183 (1), pp. 465-474. , COI: 1:CAS:528:DC%2BC2MXhvVSltb7F; Wang, X., Li, X., Li, Z., Zhang, Y., Bai, Y., Liu, H., Online coupling of in-tube solid-phase microextraction with direct analysis in real time mass spectrometry for rapid determination of triazine herbicides in water using carbon-nanotubes-incorporated polymer monolith (2014) Anal Chem, 86 (10), pp. 4739-4747. , COI: 1:CAS:528:DC%2BC2cXmsVGlt7o%3D; Fresco-Cala, B., Cárdenas, S., Valcárcel, M., Preparation and evaluation of micro and meso porous silica monoliths with embedded carbon nanoparticles for the extraction of non-polar compounds from waters (2016) J Chromatogr A, 1468, pp. 55-63. , COI: 1:CAS:528:DC%2BC28XhsFOrtr7E; Lucena, R., Cárdenas, S., Ramis-ramos, G., Valcárcel, M., Herrero-martínez, J.M., UV-polymerized butyl methacrylate monoliths with embedded carboxylic single-walled carbon nanotubes for CEC applications (2014) Anal Bioanal Chem, 406 (25), p. 6329; Fresco-Cala, B., Cárdenas, S., Herrero-Martínez, J.M., Preparation of porous methacrylate monoliths with oxidized single-walled carbon nanohorns for the extraction of nonsteroidal anti-inflammatory drugs from urine samples (2017) Microchim Acta, 184 (6), pp. 1863-1871. , COI: 1:CAS:528:DC%2BC2sXltlKrsb8%3D; Alwael, H., Connolly, D., Clarke, P., Thompson, R., Twamley, B., O'Connor, B., Paull, B., Pipette-tip selective extraction of glycoproteins with lectin modified gold nano-particles on a polymer monolithic phase (2011) Analyst, 136 (12), pp. 2619-2628. , COI: 1:CAS:528:DC%2BC3MXmslOqtL8%3D; Stachowiak, T.B., Rohr, T., Hilder, E.F., Peterson, D.S., Yi, M., Svec, F., Frechet, J.M., Fabrication of porous polymer monoliths covalently attached to the walls of channels in plastic microdevices (2003) Electrophoresis, 24 (21), pp. 3689-3693. , COI: 1:CAS:528:DC%2BD3sXpsFGjsb0%3D; Krenkova, J., Foret, F., Nanoparticle-modified monolithic pipette tips for phosphopeptide enrichment (2013) Anal Bioanal Chem, 405 (7), pp. 1-9; Ma, H., Davis, R.H., Bowman, C.N., A novel sequential photoinduced living graft polymerization (2000) Macromolecules, 33 (2), pp. 331-335. , COI: 1:CAS:528:DyaK1MXotFKgtbc%3D; Rajabi, A.A., Yamini, Y., Faraji, M., Seidi, S., Solid-phase microextraction based on cetyltrimethylammonium bromide-coated magnetic nanoparticles for determination of antidepressants from biological fluids (2013) Med Chem Res, 22 (4), pp. 1570-1577. , COI: 1:CAS:528:DC%2BC38XptFCktb8%3D; Banitaba, M.H., Davarani, S.S.H., Ahmar, H., Movahed, S.K., Application of a new fiber coating based on electrochemically reduced graphene oxide for the cold-fiber headspace solid-phase microextraction of tricyclic antidepressants (2014) J Sep Sci, 37 (9-10), pp. 1162-1169. , COI: 1:CAS:528:DC%2BC2cXmsVKrsbk%3D; Jafari, M., Sedghi, R., Ebrahimzadeh, H., A platinum wire coated with a composite consisting of poly pyrrole and poly (ɛ-caprolactone) for solid phase microextraction of the antidepressant imipramine prior to its determination via ion mobility spectrometry (2016) Microchim Acta, 183 (2), pp. 805-812. , COI: 1:CAS:528:DC%2BC2MXitFSltr%2FL; Alidoust, M., Seidi, S., Rouhollahi, A., Shanehsaz, M., In-tube electrochemically controlled solid phase microextraction of amitriptyline, imipramine and chlorpromazine from human plasma by using an indole-thiophene copolymer nanocomposite (2017) Microchim Acta, 184 (7), pp. 2473-2481. , COI: 1:CAS:528:DC%2BC2sXmvVCltrg%3D; Bagheri, H., Banihashemi, S., Zandian, F.K., Microextraction of antidepressant drugs into syringes packed with a nanocomposite consisting of polydopamine, silver nanoparticles and polypyrrole (2016) Microchim Acta, 183 (1), pp. 195-202. , COI: 1:CAS:528:DC%2BC2MXhsVequrfE; Ata, Ş., Berber, M., Çabuk, H., Akyüz, M., Optimization of magnetic extraction by experimental design methodology for the determination of antidepressants in biological samples (2015) Anal Methods, 7 (15), pp. 6231-6242. , COI: 1:CAS:528:DC%2BC2MXhtVyhtbrP; Kamaruzaman, S., Sanagi, M.M., Yahaya, N., Wan Ibrahim, W.A., Endud, S., Ibrahim, W., Nazihah, W., Magnetic micro-solid-phase extraction based on magnetite-MCM-41 with gas chromatography–mass spectrometry for the determination of antidepressant drugs in biological fluids (2017) J Sep Sci, 40 (21), pp. 4222-4233. , COI: 1:CAS:528:DC%2BC2sXhslygsrjK","correspondence_address1":"Cárdenas, S.; Departamento de Química Analítica, Campus de Rabanales, Edificio Marie Curie, Spain; email: scardenas@uco.es","publisher":"Springer-Verlag Wien","issn":"00263672","coden":"MIACA","pubmed_id":"29594510","language":"English","abbrev_source_title":"Microchim. Acta","document_type":"Article","source":"Scopus","bibtex":"@ARTICLE{Fresco-Cala2018,\nauthor={Fresco-Cala, B. and Mompó-Roselló, Ó. and Simó-Alfonso, E.F. and Cárdenas, S. and Herrero-Martínez, J.M.},\ntitle={Carbon nanotube-modified monolithic polymethacrylate pipette tips for (micro)solid-phase extraction of antidepressants from urine samples},\njournal={Microchimica Acta},\nyear={2018},\nvolume={185},\nnumber={2},\ndoi={10.1007/s00604-017-2659-4},\nart_number={127},\nnote={cited By 48},\nurl={https://www.scopus.com/inward/record.uri?eid=2-s2.0-85040985542&doi=10.1007%2fs00604-017-2659-4&partnerID=40&md5=d3f06ff857e4e4593cea694215f8fbb2},\naffiliation={Departamento de Química Analítica, Instituto Universitario de Investigación en Química Fina y Nanoquímica IUNAN, Universidad de Córdoba, Campus de Rabanales, Edificio Marie Curie, Córdoba, E-14071, Spain; Department of Analytical Chemistry, University of Valencia, Dr. Moliner 50, Burjassot, Valencia 46100, Spain},\nabstract={This work evaluates the potential of methacrylate monoliths with multi-walled carbon nanotubes incorporated into the polymeric network for the extraction of antidepressants from human urine. The method is based on a micropipette solid-phase extraction tip containing a hybrid monolithic material covalently attached to the polypropylene housing. A polymer layer made from poly(ethylene dimethacrylate) was bound to the inner surface of a polypropylene tip via UV grafting. The preparation of the monolith and the microextraction steps were optimized in terms of adsorption capacity. Limits of detection ranged from 9 to 15 μg·L−1. The average precision of the method varied between 3 and 5% (intra-tips), and from 4 to 14% (inter-tips). The accuracy of the method was evaluated through a recovery study by using spiked samples. [Figure not available: see fulltext.]. © 2018, Springer-Verlag GmbH Austria, part of Springer Nature.},\nauthor_keywords={Biological samples; Carbon nanoparticles; Drugs; Hybrid monolith; Liquid chromatography; Microextraction; Photografting process; Porous polymer; UV attachment},\nkeywords={antidepressant agent; carbon nanotube; polymethacrylic acid; polymethacrylic acid derivative, adsorption; chemistry; equipment design; human; isolation and purification; limit of detection; procedures; solid phase microextraction; urine, Adsorption; Antidepressive Agents; Equipment Design; Humans; Limit of Detection; Nanotubes, Carbon; Polymethacrylic Acids; Solid Phase Microextraction},\nchemicals_cas={polymethacrylic acid, 25087-26-7; Antidepressive Agents; Nanotubes, Carbon; polymethacrylic acid; Polymethacrylic Acids},\nreferences={Bridge, J.A., Iyengar, S., Salary, C.B., Barbe, R.P., Birmaher, B., Pincus, H.A., Ren, L., Brent, D.A., Clinical response and risk for reported suicidal ideation and suicide attempts in pediatric antidepressant treatment: a meta-analysis of randomized controlled trials (2007) JAMA, 297 (15), pp. 1683-1696. , COI: 1:CAS:528:DC%2BD2sXksVChsL4%3D; 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Lucena, R., Cárdenas, S., Ramis-ramos, G., Valcárcel, M., Herrero-martínez, J.M., UV-polymerized butyl methacrylate monoliths with embedded carboxylic single-walled carbon nanotubes for CEC applications (2014) Anal Bioanal Chem, 406 (25), p. 6329; Fresco-Cala, B., Cárdenas, S., Herrero-Martínez, J.M., Preparation of porous methacrylate monoliths with oxidized single-walled carbon nanohorns for the extraction of nonsteroidal anti-inflammatory drugs from urine samples (2017) Microchim Acta, 184 (6), pp. 1863-1871. , COI: 1:CAS:528:DC%2BC2sXltlKrsb8%3D; Alwael, H., Connolly, D., Clarke, P., Thompson, R., Twamley, B., O'Connor, B., Paull, B., Pipette-tip selective extraction of glycoproteins with lectin modified gold nano-particles on a polymer monolithic phase (2011) Analyst, 136 (12), pp. 2619-2628. , COI: 1:CAS:528:DC%2BC3MXmslOqtL8%3D; Stachowiak, T.B., Rohr, T., Hilder, E.F., Peterson, D.S., Yi, M., Svec, F., Frechet, J.M., Fabrication of porous polymer monoliths covalently attached to the walls of channels in plastic microdevices (2003) Electrophoresis, 24 (21), pp. 3689-3693. , COI: 1:CAS:528:DC%2BD3sXpsFGjsb0%3D; Krenkova, J., Foret, F., Nanoparticle-modified monolithic pipette tips for phosphopeptide enrichment (2013) Anal Bioanal Chem, 405 (7), pp. 1-9; Ma, H., Davis, R.H., Bowman, C.N., A novel sequential photoinduced living graft polymerization (2000) Macromolecules, 33 (2), pp. 331-335. , COI: 1:CAS:528:DyaK1MXotFKgtbc%3D; Rajabi, A.A., Yamini, Y., Faraji, M., Seidi, S., Solid-phase microextraction based on cetyltrimethylammonium bromide-coated magnetic nanoparticles for determination of antidepressants from biological fluids (2013) Med Chem Res, 22 (4), pp. 1570-1577. , COI: 1:CAS:528:DC%2BC38XptFCktb8%3D; Banitaba, M.H., Davarani, S.S.H., Ahmar, H., Movahed, S.K., Application of a new fiber coating based on electrochemically reduced graphene oxide for the cold-fiber headspace solid-phase microextraction of tricyclic antidepressants (2014) J Sep Sci, 37 (9-10), pp. 1162-1169. , COI: 1:CAS:528:DC%2BC2cXmsVKrsbk%3D; Jafari, M., Sedghi, R., Ebrahimzadeh, H., A platinum wire coated with a composite consisting of poly pyrrole and poly (ɛ-caprolactone) for solid phase microextraction of the antidepressant imipramine prior to its determination via ion mobility spectrometry (2016) Microchim Acta, 183 (2), pp. 805-812. , COI: 1:CAS:528:DC%2BC2MXitFSltr%2FL; Alidoust, M., Seidi, S., Rouhollahi, A., Shanehsaz, M., In-tube electrochemically controlled solid phase microextraction of amitriptyline, imipramine and chlorpromazine from human plasma by using an indole-thiophene copolymer nanocomposite (2017) Microchim Acta, 184 (7), pp. 2473-2481. , COI: 1:CAS:528:DC%2BC2sXmvVCltrg%3D; Bagheri, H., Banihashemi, S., Zandian, F.K., Microextraction of antidepressant drugs into syringes packed with a nanocomposite consisting of polydopamine, silver nanoparticles and polypyrrole (2016) Microchim Acta, 183 (1), pp. 195-202. , COI: 1:CAS:528:DC%2BC2MXhsVequrfE; Ata, Ş., Berber, M., Çabuk, H., Akyüz, M., Optimization of magnetic extraction by experimental design methodology for the determination of antidepressants in biological samples (2015) Anal Methods, 7 (15), pp. 6231-6242. , COI: 1:CAS:528:DC%2BC2MXhtVyhtbrP; Kamaruzaman, S., Sanagi, M.M., Yahaya, N., Wan Ibrahim, W.A., Endud, S., Ibrahim, W., Nazihah, W., Magnetic micro-solid-phase extraction based on magnetite-MCM-41 with gas chromatography–mass spectrometry for the determination of antidepressant drugs in biological fluids (2017) J Sep Sci, 40 (21), pp. 4222-4233. , COI: 1:CAS:528:DC%2BC2sXhslygsrjK},\ncorrespondence_address1={Cárdenas, S.; Departamento de Química Analítica, Campus de Rabanales, Edificio Marie Curie, Spain; email: scardenas@uco.es},\npublisher={Springer-Verlag Wien},\nissn={00263672},\ncoden={MIACA},\npubmed_id={29594510},\nlanguage={English},\nabbrev_source_title={Microchim. Acta},\ndocument_type={Article},\nsource={Scopus},\n}\n\n","author_short":["Fresco-Cala, B.","Mompó-Roselló, Ó.","Simó-Alfonso, E.","Cárdenas, S.","Herrero-Martínez, J."],"key":"Fresco-Cala2018","id":"Fresco-Cala2018","bibbaseid":"frescocala-momprosell-simalfonso-crdenas-herreromartnez-carbonnanotubemodifiedmonolithicpolymethacrylatepipettetipsformicrosolidphaseextractionofantidepressantsfromurinesamples-2018","role":"author","urls":{"Paper":"https://www.scopus.com/inward/record.uri?eid=2-s2.0-85040985542&doi=10.1007%2fs00604-017-2659-4&partnerID=40&md5=d3f06ff857e4e4593cea694215f8fbb2"},"keyword":["antidepressant agent; carbon nanotube; polymethacrylic acid; polymethacrylic acid derivative","adsorption; chemistry; equipment design; human; isolation and purification; limit of detection; procedures; solid phase microextraction; urine","Adsorption; Antidepressive Agents; Equipment Design; Humans; Limit of Detection; Nanotubes","Carbon; Polymethacrylic Acids; Solid Phase Microextraction"],"metadata":{"authorlinks":{}},"html":""},"bibtype":"article","biburl":"https://www.clecem.es/wp-content/uploads/2024/01/scopus.bib","dataSources":["z88YG74vvXjjYpRcn"],"keywords":["antidepressant agent; carbon nanotube; polymethacrylic acid; polymethacrylic acid derivative","adsorption; chemistry; equipment design; human; isolation and purification; limit of detection; procedures; solid phase microextraction; urine","adsorption; antidepressive agents; equipment design; humans; limit of detection; nanotubes","carbon; polymethacrylic acids; solid phase microextraction"],"search_terms":["carbon","nanotube","modified","monolithic","polymethacrylate","pipette","tips","micro","solid","phase","extraction","antidepressants","urine","samples","fresco-cala","mompó-roselló","simó-alfonso","cárdenas","herrero-martínez"],"title":"Carbon nanotube-modified monolithic polymethacrylate pipette tips for (micro)solid-phase extraction of antidepressants from urine samples","year":2018}