Morphological characterization of vanadium oxide supported on carbon-coated monoliths using AFM. Garcia-Bordeje, E, Lazaro, M., Moliner, R, Galindo, J., Sotres, J, & Baro, A. APPLIED SURFACE SCIENCE, 228(1-4):135-142, APR 30, 2004. doi abstract bibtex Vanadium has been supported on carbon-coated monoliths with three different loadings, viz. 4, 6 and 8 wt.%. The structure of vanadium catalyst has been characterized by atomic force microscopy, N-2 adsorption and XRD. All these techniques agree to indicate that vanadium is dispersed as overlayers up to 6 wt.% loadings. For higher loadings crystallites appear. The size and shape of these crystallites (12 nm average size) have been characterized by AFM. The amount of vanadium per gram of support deposited as monolayer on our carbon support can be higher than in a traditional oxide supports as, e.g. TiO2. This is a consequence of the higher surface area of carbon. The monolayer dispersion of vanadium on the carbon-coated monoliths endows this catalyst with a great potentiality to be used in reactions as, e.g. the SCR of NO at low temperature. (C) 2004 Elsevier B.V. All rights reserved.
@article{ ISI:000221367000020,
Author = {Garcia-Bordeje, E and Lazaro, MJ and Moliner, R and Galindo, JF and
Sotres, J and Baro, AM},
Title = {{Morphological characterization of vanadium oxide supported on
carbon-coated monoliths using AFM}},
Journal = {{APPLIED SURFACE SCIENCE}},
Year = {{2004}},
Volume = {{228}},
Number = {{1-4}},
Pages = {{135-142}},
Month = {{APR 30}},
Abstract = {{Vanadium has been supported on carbon-coated monoliths with three
different loadings, viz. 4, 6 and 8 wt.\%. The structure of vanadium
catalyst has been characterized by atomic force microscopy, N-2
adsorption and XRD. All these techniques agree to indicate that vanadium
is dispersed as overlayers up to 6 wt.\% loadings. For higher loadings
crystallites appear. The size and shape of these crystallites (12 nm
average size) have been characterized by AFM. The amount of vanadium per
gram of support deposited as monolayer on our carbon support can be
higher than in a traditional oxide supports as, e.g. TiO2. This is a
consequence of the higher surface area of carbon. The monolayer
dispersion of vanadium on the carbon-coated monoliths endows this
catalyst with a great potentiality to be used in reactions as, e.g. the
SCR of NO at low temperature. (C) 2004 Elsevier B.V. All rights
reserved.}},
DOI = {{10.1016/j.apsusc.2004.01.001}},
ISSN = {{0169-4332}},
EISSN = {{1873-5584}},
ResearcherID-Numbers = {{Garcia-Bordeje, Enrique/H-4187-2011
Galindo-Santos, Juan/R-4085-2018
LAZARO, MARIA JESUS/K-4585-2014
Sotres, Javier/L-1900-2013
Baro, Arturo M/C-4539-2011}},
ORCID-Numbers = {{Garcia-Bordeje, Enrique/0000-0001-8158-1270
Galindo-Santos, Juan/0000-0003-0846-4128
LAZARO, MARIA JESUS/0000-0002-4769-2564
Sotres, Javier/0000-0001-6937-3057
}},
Unique-ID = {{ISI:000221367000020}},
}
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The structure of vanadium catalyst has been characterized by atomic force microscopy, N-2 adsorption and XRD. All these techniques agree to indicate that vanadium is dispersed as overlayers up to 6 wt.% loadings. For higher loadings crystallites appear. The size and shape of these crystallites (12 nm average size) have been characterized by AFM. The amount of vanadium per gram of support deposited as monolayer on our carbon support can be higher than in a traditional oxide supports as, e.g. TiO2. This is a consequence of the higher surface area of carbon. The monolayer dispersion of vanadium on the carbon-coated monoliths endows this catalyst with a great potentiality to be used in reactions as, e.g. the SCR of NO at low temperature. (C) 2004 Elsevier B.V. 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The structure of vanadium\n catalyst has been characterized by atomic force microscopy, N-2\n adsorption and XRD. All these techniques agree to indicate that vanadium\n is dispersed as overlayers up to 6 wt.\\% loadings. For higher loadings\n crystallites appear. The size and shape of these crystallites (12 nm\n average size) have been characterized by AFM. The amount of vanadium per\n gram of support deposited as monolayer on our carbon support can be\n higher than in a traditional oxide supports as, e.g. TiO2. This is a\n consequence of the higher surface area of carbon. The monolayer\n dispersion of vanadium on the carbon-coated monoliths endows this\n catalyst with a great potentiality to be used in reactions as, e.g. the\n SCR of NO at low temperature. (C) 2004 Elsevier B.V. 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