Rhodium Dispersion in a Rh/Ce0.68Zr0.32O2 Catalyst Investigated by HRTEM and H2 Chemisorption. Gatica, J., Baker, R., Fornasiero, P., Bernal, S., Blanco, G., & Kašpar, J. Journal of Physical Chemistry B, 104(19):4667–4672, Dipartimento di Scienze Chimiche, Università di Trieste, Via Giorgieri 1, Trieste 34127, Italy, 2000. Paper abstract bibtex The effect of reduction temperature on the hydrogen adsorption and Rh dispersion in a Rh/Ce0.68Zr0.32O2 catalyst with texturally stable Ce0.68Zr0.32O2 support was investigated. Rh dispersion data were also obtained from Rh particle size analyses made using high-resolution transmission electron microscopy (HRTEM) images. Comparison of the dispersion values obtained by using the two techniques showed that H2 adsorption at -80 °C is a suitable tool for the estimation of Rh dispersion at reduction temperature, Tred, ≤500°C. For Tred > 500°C. a partial suppression of H2 chemisorption was observed. However, after a mild reoxidation and low temperature reduction, the H2 adsorption capacity of these samples was regenerated and good agreement with the HRTEM data was again obtained.
@article{Gatica20004667,
abstract = {The effect of reduction temperature on the hydrogen adsorption and Rh dispersion in a Rh/Ce0.68Zr0.32O2 catalyst with texturally stable Ce0.68Zr0.32O2 support was investigated. Rh dispersion data were also obtained from Rh particle size analyses made using high-resolution transmission electron microscopy (HRTEM) images. Comparison of the dispersion values obtained by using the two techniques showed that H2 adsorption at -80 °C is a suitable tool for the estimation of Rh dispersion at reduction temperature, Tred, ≤500°C. For Tred > 500°C. a partial suppression of H2 chemisorption was observed. However, after a mild reoxidation and low temperature reduction, the H2 adsorption capacity of these samples was regenerated and good agreement with the HRTEM data was again obtained.},
address = {Dipartimento di Scienze Chimiche, Universit\`{a} di Trieste, Via Giorgieri 1, Trieste 34127, Italy},
annote = {From Duplicate 1 ( Rhodium Dispersion in a Rh/Ce0.68Zr0.32O2 Catalyst Investigated by HRTEM and H2 Chemisorption - Gatica J.M.a Baker, R.T.b c Fornasiero P.a Bernal S.b Blanco G.b Ka\v{s}par J.a )
cited By (since 1996)44
From Duplicate 2 ( Rhodium Dispersion in a Rh/Ce0.68Zr0.32O2 Catalyst Investigated by HRTEM and H2 Chemisorption - Gatica, J.M.a; Baker, R.T.b c; Fornasiero, P.a; Bernal, S.b; Blanco, G.b; Ka\v{s}par, J.a )
cited By (since 1996)43
From Duplicate 3 ( Rhodium Dispersion in a Rh/Ce 0.68Zr 0.32O 2 Catalyst Investigated by HRTEM and H 2 Chemisorption - Gatica, J M; Baker, R T; Fornasiero, P; Bernal, S; Blanco, G; Ka\v{s}par, J )
Cited By (since 1996): 42
Export Date: 22 January 2013
Source: Scopus
CODEN: JPCBF
Language of Original Document: English
Correspondence Address: Ka\v{s}par, J.; Dipartimento di Scienze Chimiche, Universit\`{a} di Trieste, Via Giorgieri 1, Trieste 34127, Italy; email: Kaspar@univ.trieste.it
References: Anderson, J.R., (1975) Structure of Metallic Catalysts, , Accademic Press: London;
Heck, R.M., Farrauto, R.J., (1995) Catalytic Air Pollution Control. Commercial Technology, , Van Nostrand Reinhold: New York;
Kaspar, J., Fornasiero, P., Graziani, M., (1999) Catal. Today, 50, p. 285;
Taylor, K.C., (1984) Automobile Catalytic Converters. Catalysis - Science and Technology, , Anderson, J. R., Boudart, M., Eds.; Springer-Verlag: Berlin, Chapter 5;
Taylor, K.C., (1993) Catal. Rev.-Sci. Eng., 35, p. 457;
Shelef, M., Graham, G.W., (1994) Catal. Rev.-Sci. Eng., 36, p. 433;
Nunan, J.G., Robota, H.J., Cohn, M.J., Bradley, S.A., (1992) J. Catal., 133, p. 309;
Bernal, S., Calvino, J.J., Cifredo, G.A., Rodriguez-Izquierdo, J.M., Perrichon, V., Laachir, A., (1992) J. Chem. Soc. Chem. Commun., p. 460;
Bernal, S., Calvino, J.J., Cifredo, G.A., Rodriguez-Izquierdo, J.M., Perrichon, V., Laachir, A., (1992) J. Catal., 137, p. 1;
Bernal, S., Botana, F.J., Calvino, J.J., Cauqui, M.A., Cifredo, G.A., Jobacho, A., Pintado, J.M., Rodriguez-Izquierdo, J.M., (1993) J. Phys. Chem., 97, p. 4118;
Trovarelli, A., Dolcetti, G., De Leitenburg, C., Kaspar, J., Finetti, P., Santoni, A., (1992) J. Chem. Soc., Faraday Trans., 88, p. 1311;
Fornasiero, P., Kaspar, J., Graziani, M., (1997) J. Catal., 167, p. 576;
Fornasiero, P., Kaspar, J., Sergo, V., Graziani, M., (1999) J. Catal., 182, p. 56;
Bernal, S., Calvino, J.J., Cifredo, G.A., Gatica, J.M., Perez-Omil, J.A., Laachir, A., Perrichon, V., (1995) Stud. Surf. Sci. Catal., 96, p. 419;
Fornasiero, P., Hickey, N., Kaspar, J., Dossi, C., Gava, D., Graziani, M., (2000) J. Catal., 189, p. 326;
Trovarelli, A., (1996) Catat. Rev.-Sci. Eng., 38, p. 439;
Bensalem, A., Muller, J.C., Tessier, D., Bozon-Verduraz, F., (1996) J. Chem. Soc., Faraday Trans., 92, p. 3233;
Holmgren, A., Andersson, B., Duprez, D., (1999) Appl. Catal., B, 22, p. 215;
Fajardie, F., Tempere, J.F., Djega-Mariadassou, G., Blanchard, G., (1996) J. Catal., 163, p. 77;
Bernal, S., Calvino, J.J., Cauqui, M.A., Perez-Omil, J.A., Pintado, J.M., Rodriguez-Izquierdo, J.M., (1998) Appl. Catal., B, 16, p. 127;
Bernal, S., Calvino, J.J., Cauqui, M.A., Gatica, J.M., Larese, C., Omil, J.A.P., Pintado, J.M., (1999) Catal. Today, 50, p. 175;
Colon, G., Pijolat, M., Valdivieso, F., Vidal, H., Kaspar, J., Finocchio, E., Daturi, M., Bernal, S., (1998) J. Chem. Soc.Faraday Trans., 94, p. 3717;
Daturi, M., Binet, C., Lavalley, J.C., Vidai, H., Kaspar, J., Graziani, M., Blanchard, G., (1998) J. Chem. Phys., 95, p. 2048;
Colon, G., Valdivieso, F., Pijolat, M., Baker, R.T., Calvino, J.J., Bernal, S., (1999) Catal. Today, 50, p. 271;
Bernal, S., Botana, F.J., Calvino, J.J., Cifredo, G.A., Perez-Omil, J.A., (1995) Catal. Today, 23, p. 219;
Bernal, S., Blanco, G., Calvino, J.J., Cifredo, G.A., Perez-Omil, J.A., Pintado, J.M., Varo, A., (1994) Stud. Surf. Sci. Catal., 82, p. 507;
Bernal, S., Calvino, J.J., Cifredo, G.A., Laachir, A., Perrichon, V., Herrmann, J.M., (1994) Langmuir, 10, p. 717;
Badri, A., Binet, C., Lavalley, J.C., (1996) J. Chem. Soc., Faraday Trans., 92, p. 1603;
Pijolat, M., (1999), Personal communicationPfau, A., Sanz, J., Schierbaum, K.D., Gopel, W., Belzunegui, J.P., Rojo, J.M., (1996) Stud. Surf. Sci. Catal., 101, p. 931
},
author = {Gatica, JM. and Baker, RT. and Fornasiero, P. and Bernal, S. and Blanco, G. and Ka\v{s}par, J.},
issn = {10895647},
journal = {Journal of Physical Chemistry B},
number = {19},
pages = {4667--4672},
title = {{Rhodium Dispersion in a Rh/Ce0.68Zr0.32O2 Catalyst Investigated by HRTEM and H2 Chemisorption}},
url = {http://www.scopus.com/inward/record.url?eid=2-s2.0-0034682405&partnerID=40&md5=1716fe02fff14e2f6192a0fef8dbfcab https://www.scopus.com/inward/record.url?eid=2-s2.0-0034682405&partnerID=40&md5=88df7f0a12afa886519ed214c56c7303},
volume = {104},
year = {2000}
}
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Comparison of the dispersion values obtained by using the two techniques showed that H2 adsorption at -80 °C is a suitable tool for the estimation of Rh dispersion at reduction temperature, Tred, ≤500°C. For Tred > 500°C. a partial suppression of H2 chemisorption was observed. However, after a mild reoxidation and low temperature reduction, the H2 adsorption capacity of these samples was regenerated and good agreement with the HRTEM data was again obtained.","address":"Dipartimento di Scienze Chimiche, Università di Trieste, Via Giorgieri 1, Trieste 34127, Italy","annote":"From Duplicate 1 ( Rhodium Dispersion in a Rh/Ce0.68Zr0.32O2 Catalyst Investigated by HRTEM and H2 Chemisorption - Gatica J.M.a Baker, R.T.b c Fornasiero P.a Bernal S.b Blanco G.b Kašpar J.a ) cited By (since 1996)44 From Duplicate 2 ( Rhodium Dispersion in a Rh/Ce0.68Zr0.32O2 Catalyst Investigated by HRTEM and H2 Chemisorption - Gatica, J.M.a; Baker, R.T.b c; Fornasiero, P.a; Bernal, S.b; Blanco, G.b; Kašpar, J.a ) cited By (since 1996)43 From Duplicate 3 ( Rhodium Dispersion in a Rh/Ce 0.68Zr 0.32O 2 Catalyst Investigated by HRTEM and H 2 Chemisorption - Gatica, J M; Baker, R T; Fornasiero, P; Bernal, S; Blanco, G; Kašpar, J ) Cited By (since 1996): 42 Export Date: 22 January 2013 Source: Scopus CODEN: JPCBF Language of Original Document: English Correspondence Address: Kašpar, J.; Dipartimento di Scienze Chimiche, Università di Trieste, Via Giorgieri 1, Trieste 34127, Italy; email: Kaspar@univ.trieste.it References: Anderson, J.R., (1975) Structure of Metallic Catalysts, , Accademic Press: London; Heck, R.M., Farrauto, R.J., (1995) Catalytic Air Pollution Control. Commercial Technology, , Van Nostrand Reinhold: New York; Kaspar, J., Fornasiero, P., Graziani, M., (1999) Catal. Today, 50, p. 285; Taylor, K.C., (1984) Automobile Catalytic Converters. Catalysis - Science and Technology, , Anderson, J. R., Boudart, M., Eds.; Springer-Verlag: Berlin, Chapter 5; Taylor, K.C., (1993) Catal. Rev.-Sci. Eng., 35, p. 457; Shelef, M., Graham, G.W., (1994) Catal. Rev.-Sci. Eng., 36, p. 433; Nunan, J.G., Robota, H.J., Cohn, M.J., Bradley, S.A., (1992) J. Catal., 133, p. 309; Bernal, S., Calvino, J.J., Cifredo, G.A., Rodriguez-Izquierdo, J.M., Perrichon, V., Laachir, A., (1992) J. Chem. Soc. Chem. Commun., p. 460; Bernal, S., Calvino, J.J., Cifredo, G.A., Rodriguez-Izquierdo, J.M., Perrichon, V., Laachir, A., (1992) J. Catal., 137, p. 1; Bernal, S., Botana, F.J., Calvino, J.J., Cauqui, M.A., Cifredo, G.A., Jobacho, A., Pintado, J.M., Rodriguez-Izquierdo, J.M., (1993) J. Phys. Chem., 97, p. 4118; Trovarelli, A., Dolcetti, G., De Leitenburg, C., Kaspar, J., Finetti, P., Santoni, A., (1992) J. Chem. Soc., Faraday Trans., 88, p. 1311; Fornasiero, P., Kaspar, J., Graziani, M., (1997) J. Catal., 167, p. 576; Fornasiero, P., Kaspar, J., Sergo, V., Graziani, M., (1999) J. Catal., 182, p. 56; Bernal, S., Calvino, J.J., Cifredo, G.A., Gatica, J.M., Perez-Omil, J.A., Laachir, A., Perrichon, V., (1995) Stud. Surf. Sci. Catal., 96, p. 419; Fornasiero, P., Hickey, N., Kaspar, J., Dossi, C., Gava, D., Graziani, M., (2000) J. Catal., 189, p. 326; Trovarelli, A., (1996) Catat. Rev.-Sci. Eng., 38, p. 439; Bensalem, A., Muller, J.C., Tessier, D., Bozon-Verduraz, F., (1996) J. Chem. Soc., Faraday Trans., 92, p. 3233; Holmgren, A., Andersson, B., Duprez, D., (1999) Appl. Catal., B, 22, p. 215; Fajardie, F., Tempere, J.F., Djega-Mariadassou, G., Blanchard, G., (1996) J. Catal., 163, p. 77; Bernal, S., Calvino, J.J., Cauqui, M.A., Perez-Omil, J.A., Pintado, J.M., Rodriguez-Izquierdo, J.M., (1998) Appl. Catal., B, 16, p. 127; Bernal, S., Calvino, J.J., Cauqui, M.A., Gatica, J.M., Larese, C., Omil, J.A.P., Pintado, J.M., (1999) Catal. Today, 50, p. 175; Colon, G., Pijolat, M., Valdivieso, F., Vidal, H., Kaspar, J., Finocchio, E., Daturi, M., Bernal, S., (1998) J. Chem. Soc.Faraday Trans., 94, p. 3717; Daturi, M., Binet, C., Lavalley, J.C., Vidai, H., Kaspar, J., Graziani, M., Blanchard, G., (1998) J. Chem. Phys., 95, p. 2048; Colon, G., Valdivieso, F., Pijolat, M., Baker, R.T., Calvino, J.J., Bernal, S., (1999) Catal. Today, 50, p. 271; Bernal, S., Botana, F.J., Calvino, J.J., Cifredo, G.A., Perez-Omil, J.A., (1995) Catal. Today, 23, p. 219; Bernal, S., Blanco, G., Calvino, J.J., Cifredo, G.A., Perez-Omil, J.A., Pintado, J.M., Varo, A., (1994) Stud. Surf. Sci. Catal., 82, p. 507; Bernal, S., Calvino, J.J., Cifredo, G.A., Laachir, A., Perrichon, V., Herrmann, J.M., (1994) Langmuir, 10, p. 717; Badri, A., Binet, C., Lavalley, J.C., (1996) J. Chem. Soc., Faraday Trans., 92, p. 1603; Pijolat, M., (1999), Personal communicationPfau, A., Sanz, J., Schierbaum, K.D., Gopel, W., Belzunegui, J.P., Rojo, J.M., (1996) Stud. Surf. Sci. Catal., 101, p. 931 ","author":[{"propositions":[],"lastnames":["Gatica"],"firstnames":["JM."],"suffixes":[]},{"propositions":[],"lastnames":["Baker"],"firstnames":["RT."],"suffixes":[]},{"propositions":[],"lastnames":["Fornasiero"],"firstnames":["P."],"suffixes":[]},{"propositions":[],"lastnames":["Bernal"],"firstnames":["S."],"suffixes":[]},{"propositions":[],"lastnames":["Blanco"],"firstnames":["G."],"suffixes":[]},{"propositions":[],"lastnames":["Kašpar"],"firstnames":["J."],"suffixes":[]}],"issn":"10895647","journal":"Journal of Physical Chemistry B","number":"19","pages":"4667–4672","title":"Rhodium Dispersion in a Rh/Ce0.68Zr0.32O2 Catalyst Investigated by HRTEM and H2 Chemisorption","url":"http://www.scopus.com/inward/record.url?eid=2-s2.0-0034682405&partnerID=40&md5=1716fe02fff14e2f6192a0fef8dbfcab https://www.scopus.com/inward/record.url?eid=2-s2.0-0034682405&partnerID=40&md5=88df7f0a12afa886519ed214c56c7303","volume":"104","year":"2000","bibtex":"@article{Gatica20004667,\nabstract = {The effect of reduction temperature on the hydrogen adsorption and Rh dispersion in a Rh/Ce0.68Zr0.32O2 catalyst with texturally stable Ce0.68Zr0.32O2 support was investigated. Rh dispersion data were also obtained from Rh particle size analyses made using high-resolution transmission electron microscopy (HRTEM) images. Comparison of the dispersion values obtained by using the two techniques showed that H2 adsorption at -80 °C is a suitable tool for the estimation of Rh dispersion at reduction temperature, Tred, ≤500°C. For Tred > 500°C. a partial suppression of H2 chemisorption was observed. However, after a mild reoxidation and low temperature reduction, the H2 adsorption capacity of these samples was regenerated and good agreement with the HRTEM data was again obtained.},\naddress = {Dipartimento di Scienze Chimiche, Universit\\`{a} di Trieste, Via Giorgieri 1, Trieste 34127, Italy},\nannote = {From Duplicate 1 ( Rhodium Dispersion in a Rh/Ce0.68Zr0.32O2 Catalyst Investigated by HRTEM and H2 Chemisorption - Gatica J.M.a Baker, R.T.b c Fornasiero P.a Bernal S.b Blanco G.b Ka\\v{s}par J.a )\n\ncited By (since 1996)44\n\nFrom Duplicate 2 ( Rhodium Dispersion in a Rh/Ce0.68Zr0.32O2 Catalyst Investigated by HRTEM and H2 Chemisorption - Gatica, J.M.a; Baker, R.T.b c; Fornasiero, P.a; Bernal, S.b; Blanco, G.b; Ka\\v{s}par, J.a )\n\ncited By (since 1996)43\n\n\nFrom Duplicate 3 ( Rhodium Dispersion in a Rh/Ce 0.68Zr 0.32O 2 Catalyst Investigated by HRTEM and H 2 Chemisorption - Gatica, J M; Baker, R T; Fornasiero, P; Bernal, S; Blanco, G; Ka\\v{s}par, J )\n\nCited By (since 1996): 42\n \nExport Date: 22 January 2013\n \nSource: Scopus\n \nCODEN: JPCBF\n \nLanguage of Original Document: English\n \nCorrespondence Address: Ka\\v{s}par, J.; Dipartimento di Scienze Chimiche, Universit\\`{a} di Trieste, Via Giorgieri 1, Trieste 34127, Italy; email: Kaspar@univ.trieste.it\n \nReferences: Anderson, J.R., (1975) Structure of Metallic Catalysts, , Accademic Press: London; \nHeck, R.M., Farrauto, R.J., (1995) Catalytic Air Pollution Control. Commercial Technology, , Van Nostrand Reinhold: New York; \nKaspar, J., Fornasiero, P., Graziani, M., (1999) Catal. Today, 50, p. 285; \nTaylor, K.C., (1984) Automobile Catalytic Converters. Catalysis - Science and Technology, , Anderson, J. R., Boudart, M., Eds.; Springer-Verlag: Berlin, Chapter 5; \nTaylor, K.C., (1993) Catal. Rev.-Sci. Eng., 35, p. 457; \nShelef, M., Graham, G.W., (1994) Catal. Rev.-Sci. Eng., 36, p. 433; \nNunan, J.G., Robota, H.J., Cohn, M.J., Bradley, S.A., (1992) J. Catal., 133, p. 309; \nBernal, S., Calvino, J.J., Cifredo, G.A., Rodriguez-Izquierdo, J.M., Perrichon, V., Laachir, A., (1992) J. Chem. Soc. Chem. Commun., p. 460; \nBernal, S., Calvino, J.J., Cifredo, G.A., Rodriguez-Izquierdo, J.M., Perrichon, V., Laachir, A., (1992) J. Catal., 137, p. 1; \nBernal, S., Botana, F.J., Calvino, J.J., Cauqui, M.A., Cifredo, G.A., Jobacho, A., Pintado, J.M., Rodriguez-Izquierdo, J.M., (1993) J. Phys. Chem., 97, p. 4118; \nTrovarelli, A., Dolcetti, G., De Leitenburg, C., Kaspar, J., Finetti, P., Santoni, A., (1992) J. Chem. Soc., Faraday Trans., 88, p. 1311; \nFornasiero, P., Kaspar, J., Graziani, M., (1997) J. Catal., 167, p. 576; \nFornasiero, P., Kaspar, J., Sergo, V., Graziani, M., (1999) J. Catal., 182, p. 56; \nBernal, S., Calvino, J.J., Cifredo, G.A., Gatica, J.M., Perez-Omil, J.A., Laachir, A., Perrichon, V., (1995) Stud. Surf. Sci. Catal., 96, p. 419; \nFornasiero, P., Hickey, N., Kaspar, J., Dossi, C., Gava, D., Graziani, M., (2000) J. Catal., 189, p. 326; \nTrovarelli, A., (1996) Catat. Rev.-Sci. Eng., 38, p. 439; \nBensalem, A., Muller, J.C., Tessier, D., Bozon-Verduraz, F., (1996) J. Chem. Soc., Faraday Trans., 92, p. 3233; \nHolmgren, A., Andersson, B., Duprez, D., (1999) Appl. Catal., B, 22, p. 215; \nFajardie, F., Tempere, J.F., Djega-Mariadassou, G., Blanchard, G., (1996) J. Catal., 163, p. 77; \nBernal, S., Calvino, J.J., Cauqui, M.A., Perez-Omil, J.A., Pintado, J.M., Rodriguez-Izquierdo, J.M., (1998) Appl. Catal., B, 16, p. 127; \nBernal, S., Calvino, J.J., Cauqui, M.A., Gatica, J.M., Larese, C., Omil, J.A.P., Pintado, J.M., (1999) Catal. Today, 50, p. 175; \nColon, G., Pijolat, M., Valdivieso, F., Vidal, H., Kaspar, J., Finocchio, E., Daturi, M., Bernal, S., (1998) J. Chem. Soc.Faraday Trans., 94, p. 3717; \nDaturi, M., Binet, C., Lavalley, J.C., Vidai, H., Kaspar, J., Graziani, M., Blanchard, G., (1998) J. Chem. Phys., 95, p. 2048; \nColon, G., Valdivieso, F., Pijolat, M., Baker, R.T., Calvino, J.J., Bernal, S., (1999) Catal. Today, 50, p. 271; \nBernal, S., Botana, F.J., Calvino, J.J., Cifredo, G.A., Perez-Omil, J.A., (1995) Catal. Today, 23, p. 219; \nBernal, S., Blanco, G., Calvino, J.J., Cifredo, G.A., Perez-Omil, J.A., Pintado, J.M., Varo, A., (1994) Stud. Surf. Sci. Catal., 82, p. 507; \nBernal, S., Calvino, J.J., Cifredo, G.A., Laachir, A., Perrichon, V., Herrmann, J.M., (1994) Langmuir, 10, p. 717; \nBadri, A., Binet, C., Lavalley, J.C., (1996) J. Chem. Soc., Faraday Trans., 92, p. 1603; \nPijolat, M., (1999), Personal communicationPfau, A., Sanz, J., Schierbaum, K.D., Gopel, W., Belzunegui, J.P., Rojo, J.M., (1996) Stud. Surf. Sci. 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