Multiple-Quantum Magic-Angle Spinning: High-Resolution Solid State NMR Spectroscopy of Half-Integer Quadrupolar Nuclei. Goldbourt, A. & Madhu, P. K Monatshefte f?r Chemie / Chemical Monthly, 133(12):1497–1534, December, 2002.
Multiple-Quantum Magic-Angle Spinning: High-Resolution Solid State NMR Spectroscopy of Half-Integer Quadrupolar Nuclei [link]Paper  doi  abstract   bibtex   
Summary. Experimental and theoretical aspects of the multiple-quantum magic-angle spinning experiment (MQMAS) are discussed in this review. The significance of this experiment, introduced by Frydman and Harwood, is in its ability to provide high-resolution NMR spectra of half-integer quadrupolar nuclei (I greater than or equal to 3/2). This technique has proved to be useful in various systems ranging from inorganic materials to biological samples. This review addresses the development of various pulse schemes aimed at improving the signal-to-noise ratio and anisotropic lineshapes. Representative spectra are shown to underscore the importance and applications of the MQMAS experiment.
@article{Goldbourt2002,
	title = {Multiple-{Quantum} {Magic}-{Angle} {Spinning}: {High}-{Resolution} {Solid} {State} {NMR} {Spectroscopy} of {Half}-{Integer} {Quadrupolar} {Nuclei}},
	volume = {133},
	issn = {00269247},
	url = {http://link.springer.com/10.1007/s00706-002-0502-y},
	doi = {10.1007/s00706-002-0502-y},
	abstract = {Summary. Experimental and theoretical aspects of the multiple-quantum magic-angle spinning experiment (MQMAS) are discussed in this review. The significance of this experiment, introduced by Frydman and Harwood, is in its ability to provide high-resolution NMR spectra of half-integer quadrupolar nuclei (I greater than or equal to 3/2). This technique has proved to be useful in various systems ranging from inorganic materials to biological samples. This review addresses the development of various pulse schemes aimed at improving the signal-to-noise ratio and anisotropic lineshapes. Representative spectra are shown to underscore the importance and applications of the MQMAS experiment.},
	number = {12},
	journal = {Monatshefte f?r Chemie / Chemical Monthly},
	author = {Goldbourt, Amir and Madhu, Perunthiruthy K},
	month = dec,
	year = {2002},
	keywords = {Amplitude modulation, MQMAS, NMR spectroscopy, Quadrupolar nuclei, Solid state},
	pages = {1497--1534},
}

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