Molecular-level characterization of the structure and the surface chemistry of periodic mesoporous organosilicates using DNP-surface enhanced NMR spectroscopy. Grüning, W. R, Rossini, A. J, Zagdoun, A., Gajan, D., Lesage, A., Emsley, L., & Copéret, C. Physical chemistry chemical physics : PCCP, 15:13270–13274, 2013.
Paper doi abstract bibtex We present the molecular level characterization of a phenylpyridine-based periodic mesoporous organosilicate and its post-functionalized organometallic derivatives through the fast acquisition of high quality natural isotopic abundance 1D (13)C, (15)N, and (29)Si and 2D (1)H-(13)C and (1)H-(29)Si solid-state NMR spectra enhanced with dynamic nuclear polarization.
@article{Gruning2013,
title = {Molecular-level characterization of the structure and the surface chemistry of periodic mesoporous organosilicates using {DNP}-surface enhanced {NMR} spectroscopy.},
volume = {15},
issn = {1463-9084},
url = {http://www.ncbi.nlm.nih.gov/pubmed/23440402},
doi = {10.1039/c3cp00026e},
abstract = {We present the molecular level characterization of a phenylpyridine-based periodic mesoporous organosilicate and its post-functionalized organometallic derivatives through the fast acquisition of high quality natural isotopic abundance 1D (13)C, (15)N, and (29)Si and 2D (1)H-(13)C and (1)H-(29)Si solid-state NMR spectra enhanced with dynamic nuclear polarization.},
journal = {Physical chemistry chemical physics : PCCP},
author = {Grüning, Wolfram R and Rossini, Aaron J and Zagdoun, Alexandre and Gajan, David and Lesage, Anne and Emsley, Lyndon and Copéret, Christophe},
year = {2013},
pmid = {23440402},
keywords = {\#nosource, Magnetic Resonance Spectroscopy, Magnetic Resonance Spectroscopy: methods, Molecular Structure, Organosilicon Compounds, Organosilicon Compounds: chemistry, Particle Size, Porosity, Surface Properties},
pages = {13270--13274},
}
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