Frequency dependence of heat capacity of the Pd 40 Ni 10 Cu 30 P 20 amorphous alloy by temperature-modulated calorimetry. Hu, X. & Li, Y. Technical Report 2000.
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Paper Website abstract bibtex The frequency dependence of the heat capacity in the glass-transition region of Pd 40 Ni 10 Cu 30 P 20 was studied by temperature-modulated dierential scanning calorimetry (TMDSC) during slow heating and cooling. Such data for low frequencies between 0.1 and 0.01 Hz are not available, especially for metallic glasses. A crossover between mixed static/ dynamic and purely dynamic response signals was observed for the lowest frequencies between 1/80 and 1/100 s À1 , which allows a direct determination of the average relaxation time at a given cooling rate during the static glass transition. Further, these results were used to evaluate the experimental parameters necessary to truly separate the static and dynamic response in low-frequency modulation calorimetry experiments to obtain the moduli of the dynamic speci®c heat. Ó
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title = {Frequency dependence of heat capacity of the Pd 40 Ni 10 Cu 30 P 20 amorphous alloy by temperature-modulated calorimetry},
type = {techreport},
year = {2000},
keywords = {1999,calorimetry,copper,cu,glass,modulated,ni,nickel,p,palladium,pd,temperature,transition},
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abstract = {The frequency dependence of the heat capacity in the glass-transition region of Pd 40 Ni 10 Cu 30 P 20 was studied by temperature-modulated dierential scanning calorimetry (TMDSC) during slow heating and cooling. Such data for low frequencies between 0.1 and 0.01 Hz are not available, especially for metallic glasses. A crossover between mixed static/ dynamic and purely dynamic response signals was observed for the lowest frequencies between 1/80 and 1/100 s À1 , which allows a direct determination of the average relaxation time at a given cooling rate during the static glass transition. Further, these results were used to evaluate the experimental parameters necessary to truly separate the static and dynamic response in low-frequency modulation calorimetry experiments to obtain the moduli of the dynamic speci®c heat. Ó},
bibtype = {techreport},
author = {Hu, X and Li, Y}
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