Novel and Efficient Methods for the Synthesis of Symmetrical Trisulfides. Kertmen, A., Lach, S., Rachon, J., & Witt, D. Synthesis-Stuttgart, May, 2009. WOS:000266334000006
Novel and Efficient Methods for the Synthesis of Symmetrical Trisulfides [link]Paper  abstract   bibtex   
We have developed convenient methods for the synthesis of symmetrical trisulfides under mild conditions in very good yields. The described methods are based oil the straightforward preparation of (5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorin-2-yl)disulfanyl derivatives from readily available 5,5-dimethyl-2-sulfanyl-2-thioxo-1,3,2-dioxaphosphorinane or bis(5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinan-2-yl) disulfide. The symmetrical trisulfides can be obtained from aliphatic and aromatic thiols and also L-cysteine derivatives.
@article{ kertmen_novel_2009,
  title = {Novel and Efficient Methods for the Synthesis of Symmetrical Trisulfides},
  issn = {0039-7881},
  url = {http://dx.doi.org/10.1055/s-0028-1088161},
  abstract = {We have developed convenient methods for the synthesis of symmetrical trisulfides under mild conditions in very good yields. The described methods are based oil the straightforward preparation of (5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorin-2-yl)disulfanyl derivatives from readily available 5,5-dimethyl-2-sulfanyl-2-thioxo-1,3,2-dioxaphosphorinane or bis(5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinan-2-yl) disulfide. The symmetrical trisulfides can be obtained from aliphatic and aromatic thiols and also L-cysteine derivatives.},
  number = {9},
  journal = {Synthesis-Stuttgart},
  author = {Kertmen, Ahmet and Lach, Slawomir and Rachon, Janusz and Witt, Dariusz},
  month = {May},
  year = {2009},
  note = {{WOS:000266334000006}},
  pages = {1459--1462}
}

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