@article{ konieczka_calibration_1996,
  title = {Calibration of the thermal desorption gas chromatography mass spectrometry system using standards generated in the process of thermal decomposition of chemically modified silica gel},
  volume = {742},
  issn = {0021-9673},
  url = {http://dx.doi.org/10.1016/0021-9673(96)00316-0},
  doi = {<Go to ISI>://WOS:A1996VH55600016},
  abstract = {A calibration method for the thermal desorption gas chromatographic-mass spectrometric ({TD-GC-MS)} determination of n-propanethiol based on a gas standard mixture generated in the process of thermal decomposition of chemically modified silica gel is proposed. The experimental results indicated that the total amount of n-propanethiol liberated from unit mass of the gel did not depend on the total mass of the gel used. A calibration curve for the {TD-GC-MS} system for n-propanethiol, determined for the relationship between the mass of n-propanethiol and the mass of the modified silica gel used, was found by a linear regression method and was characterized by a correlation coefficient r=0.99. This means that the amounts of liberated n-propanethiol are directly proportional to the mass of the modified gel used within the examined range of masses of silica gel samples. Consequently, the amount of the analyte (n-propanethiol) can be determined on the basis of mass of silica gel used and hence the modified silica gel can be treated as a standard of the liberated component (n-propanethiol in this case).},
  number = {1-2},
  journal = {Journal of Chromatography A},
  author = {Konieczka, P. and Wolska, L. and Luboch, E. and Namiesnik, J. and Przyjazny, A. and Biernat, J. F.},
  year = {1996},
  pages = {175--179}
}

{"_id":{"_str":"5347aad286fcaed03b0000d0"},"__v":1,"authorIDs":[],"author_short":["Konieczka, P.","Wolska, L.","Luboch, E.","Namiesnik, J.","Przyjazny, A.","Biernat, J.<nbsp>F."],"bibbaseid":"konieczka-wolska-luboch-namiesnik-przyjazny-biernat-calibrationofthethermaldesorptiongaschromatographymassspectrometrysystemusingstandardsgeneratedintheprocessofthermaldecompositionofchemicallymodifiedsilicagel-1996","bibdata":{"downloads":0,"bibbaseid":"konieczka-wolska-luboch-namiesnik-przyjazny-biernat-calibrationofthethermaldesorptiongaschromatographymassspectrometrysystemusingstandardsgeneratedintheprocessofthermaldecompositionofchemicallymodifiedsilicagel-1996","urls":{"Paper":"http://dx.doi.org/10.1016/0021-9673(96)00316-0"},"role":"author","year":"1996","volume":"742","url":"http://dx.doi.org/10.1016/0021-9673(96)00316-0","type":"article","title":"Calibration of the thermal desorption gas chromatography mass spectrometry system using standards generated in the process of thermal decomposition of chemically modified silica gel","pages":"175--179","number":"1-2","key":"konieczka_calibration_1996","journal":"Journal of Chromatography A","issn":"0021-9673","id":"konieczka_calibration_1996","doi":"<Go to ISI>://WOS:A1996VH55600016","bibtype":"article","bibtex":"@article{ konieczka_calibration_1996,\n title = {Calibration of the thermal desorption gas chromatography mass spectrometry system using standards generated in the process of thermal decomposition of chemically modified silica gel},\n volume = {742},\n issn = {0021-9673},\n url = {http://dx.doi.org/10.1016/0021-9673(96)00316-0},\n doi = {<Go to ISI>://WOS:A1996VH55600016},\n abstract = {A calibration method for the thermal desorption gas chromatographic-mass spectrometric ({TD-GC-MS)} determination of n-propanethiol based on a gas standard mixture generated in the process of thermal decomposition of chemically modified silica gel is proposed. The experimental results indicated that the total amount of n-propanethiol liberated from unit mass of the gel did not depend on the total mass of the gel used. A calibration curve for the {TD-GC-MS} system for n-propanethiol, determined for the relationship between the mass of n-propanethiol and the mass of the modified silica gel used, was found by a linear regression method and was characterized by a correlation coefficient r=0.99. This means that the amounts of liberated n-propanethiol are directly proportional to the mass of the modified gel used within the examined range of masses of silica gel samples. Consequently, the amount of the analyte (n-propanethiol) can be determined on the basis of mass of silica gel used and hence the modified silica gel can be treated as a standard of the liberated component (n-propanethiol in this case).},\n number = {1-2},\n journal = {Journal of Chromatography A},\n author = {Konieczka, P. and Wolska, L. and Luboch, E. and Namiesnik, J. and Przyjazny, A. and Biernat, J. F.},\n year = {1996},\n pages = {175--179}\n}","author_short":["Konieczka, P.","Wolska, L.","Luboch, E.","Namiesnik, J.","Przyjazny, A.","Biernat, J.<nbsp>F."],"author":["Konieczka, P.","Wolska, L.","Luboch, E.","Namiesnik, J.","Przyjazny, A.","Biernat, J. F."],"abstract":"A calibration method for the thermal desorption gas chromatographic-mass spectrometric (TD-GC-MS) determination of n-propanethiol based on a gas standard mixture generated in the process of thermal decomposition of chemically modified silica gel is proposed. The experimental results indicated that the total amount of n-propanethiol liberated from unit mass of the gel did not depend on the total mass of the gel used. A calibration curve for the TD-GC-MS system for n-propanethiol, determined for the relationship between the mass of n-propanethiol and the mass of the modified silica gel used, was found by a linear regression method and was characterized by a correlation coefficient r=0.99. This means that the amounts of liberated n-propanethiol are directly proportional to the mass of the modified gel used within the examined range of masses of silica gel samples. Consequently, the amount of the analyte (n-propanethiol) can be determined on the basis of mass of silica gel used and hence the modified silica gel can be treated as a standard of the liberated component (n-propanethiol in this case)."},"bibtype":"article","biburl":"https://api.zotero.org/users/1240136/collections/D3IKI755/items?key=d8koCcMiuZcPhEzxkKFLW2Lc&format=bibtex&limit=100","downloads":0,"keywords":[],"search_terms":["calibration","thermal","desorption","gas","chromatography","mass","spectrometry","system","using","standards","generated","process","thermal","decomposition","chemically","modified","silica","gel","konieczka","wolska","luboch","namiesnik","przyjazny","biernat"],"title":"Calibration of the thermal desorption gas chromatography mass spectrometry system using standards generated in the process of thermal decomposition of chemically modified silica gel","year":1996,"dataSources":["2McnXGMueEZ47uPFA"]}