Sensitive absorptive refocused scalar correlation NMR spectroscopy in solids.

Sensitive absorptive refocused scalar correlation NMR spectroscopy in solids. Lee, D., Struppe, J., Elliott, D. W, Mueller, L. J, & Titman, J. J Physical chemistry chemical physics : PCCP, 11(18):3547–53, May, 2009.

Paper doi abstract bibtex

A new two-dimensional NMR experiment is described which is suitable for obtaining magic angle spinning (MAS) scalar correlation spectra in solids. The new experiment has several advantages, including increased cross peak intensities, coupled with good suppression of the diagonal. Its utility is demonstrated via assignments of the carbon-13 MAS spectra of progesterone at natural abundance and of the polymer phase of 50%-U-13C-CsC60.

@article{Lee2009a,
	title = {Sensitive absorptive refocused scalar correlation {NMR} spectroscopy in solids.},
	volume = {11},
	issn = {1463-9076},
	url = {http://www.ncbi.nlm.nih.gov/pubmed/19421560},
	doi = {10.1039/b818867j},
	abstract = {A new two-dimensional NMR experiment is described which is suitable for obtaining magic angle spinning (MAS) scalar correlation spectra in solids. The new experiment has several advantages, including increased cross peak intensities, coupled with good suppression of the diagonal. Its utility is demonstrated via assignments of the carbon-13 MAS spectra of progesterone at natural abundance and of the polymer phase of 50\%-U-13C-CsC60.},
	number = {18},
	urldate = {2013-12-18},
	journal = {Physical chemistry chemical physics : PCCP},
	author = {Lee, Daniel and Struppe, Jochem and Elliott, Douglas W and Mueller, Leonard J and Titman, Jeremy J},
	month = may,
	year = {2009},
	pmid = {19421560},
	pages = {3547--53},
}

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