13- and 26-membered crown ethers with azo and azoxy subunits in the macrocycle. Template effect in reductive macrocyclization. X-ray structure of 26-membered crown ether with two azoxy subunits. Luboch, E., Biernat, J. F., Dvorkin, A. A., & Simonov, Y. A. Polish Journal of Chemistry, 70(2):202--210, 1996. doi abstract bibtex The effect of sodium versus potassium stannite reduction of bis(2-nitrophenoxy)-3-oxapentane on ratio of 13-membered azo- and azoxycrown ether formation has been studied. Generation of 26-membered di-azo, azoazoxy and di-azoxy compounds in the presence of potassium as a template has been found. The X-ray structure of the 26-membered crown ether with two azoxy subunits in the macrocycle has been presented.
@article{ luboch_13-_1996,
title = {13- and 26-membered crown ethers with azo and azoxy subunits in the macrocycle. Template effect in reductive macrocyclization. X-ray structure of 26-membered crown ether with two azoxy subunits},
volume = {70},
issn = {0137-5083},
doi = {<Go to ISI>://WOS:A1996TT95100009},
abstract = {The effect of sodium versus potassium stannite reduction of bis(2-nitrophenoxy)-3-oxapentane on ratio of 13-membered azo- and azoxycrown ether formation has been studied. Generation of 26-membered di-azo, azoazoxy and di-azoxy compounds in the presence of potassium as a template has been found. The X-ray structure of the 26-membered crown ether with two azoxy subunits in the macrocycle has been presented.},
number = {2},
journal = {Polish Journal of Chemistry},
author = {Luboch, E. and Biernat, J. F. and Dvorkin, A. A. and Simonov, Y. A.},
year = {1996},
pages = {202--210}
}
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