Determination of trace elements in ambient aerosol samples. Pekney, N., J. & Davidson, C., I. Anal. Chim. Acta, 540:269-277, 2005. abstract bibtex A microwave-assisted digestion procedure using HNO3,
HF, and H2O2 has been developed for analysis of elements in ambient
particulate matter (PM). The samples are collected on cellulose
filters and analyzed by inductively coupled plasma mass
spectrometry (ICP-MS). The ICP-MS is calibrated with external
standards, and recovery of analytes is tested with NIST SRM 1648
Urban Dust. This method has been used to quantify the airborne
concentrations of a large number of elements, including Ag, As, Ba,
Be, Ca, Cd, Ce, Co, Cr, Cs, Cu, Fe, Ga, K, Li, Mg, Mn, Mo, Ni, Pb,
Rb, Se, Sb, Sr, Ti, Tl, V, and Zn. For the majority of these
elements, recovery of the NIST SRM is within 15% of the certified
values. (c) 2005 Elsevier B.V. All rights reserved.
C1 Carnegie Mellon Univ, Dept Civil & Environm Engn, Pittsburgh,
PA 15213 USA.
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title = {Determination of trace elements in ambient aerosol samples},
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year = {2005},
pages = {269-277},
volume = {540},
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abstract = {A microwave-assisted digestion procedure using HNO3,
HF, and H2O2 has been developed for analysis of elements in ambient
particulate matter (PM). The samples are collected on cellulose
filters and analyzed by inductively coupled plasma mass
spectrometry (ICP-MS). The ICP-MS is calibrated with external
standards, and recovery of analytes is tested with NIST SRM 1648
Urban Dust. This method has been used to quantify the airborne
concentrations of a large number of elements, including Ag, As, Ba,
Be, Ca, Cd, Ce, Co, Cr, Cs, Cu, Fe, Ga, K, Li, Mg, Mn, Mo, Ni, Pb,
Rb, Se, Sb, Sr, Ti, Tl, V, and Zn. For the majority of these
elements, recovery of the NIST SRM is within 15% of the certified
values. (c) 2005 Elsevier B.V. All rights reserved.
C1 Carnegie Mellon Univ, Dept Civil & Environm Engn, Pittsburgh,
PA 15213 USA.},
bibtype = {article},
author = {Pekney, N J and Davidson, C I},
journal = {Anal. Chim. Acta}
}
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