Combined HREM and HAADF scanning transmission electron microscopy: A powerful tool for investigating structural changes in thermally aged Ceria-Zirconia mixed oxides. Pérez-Omil, J., Bernal, S., Calvino, J., Hernández-Garrido, J., Mira, C., Rodríguez-Luque, M., Erni, R., & Browning, N. Chemistry of Materials, 17(17):4282–4285, Departamento de Ciencia de los Maienales e Ingenieria Metalurgica y Quimica Inorganica, Facultad de Ciencias, Campus Puerto Real, 11510 Cádiz, Spain, 2005.
Paper abstract bibtex The technique of combined high-resolution transmission electron microscopy (HRTEM) and high-angle annular dark field (HAADF) scanning electron microscopy for structural changes in thermally aged Ceria-Zirconia mixed oxides is investigated. The combined application of HRTEM and HAADF technique has allowed to interpret the superstructure contrasts observed in the HRTEM images of a cycled ceria-zirconia mixed oxide. It was found that the approach offers a powerful tool for characterizing structural rearrangements occurring in the cationic sublattice of these materials. It was also found that the approach allows to detect these structural effects at a nanoscale and earlier stages than those required by macroscopic techniques.
@article{Perez-Omil2005,
abstract = {The technique of combined high-resolution transmission electron microscopy (HRTEM) and high-angle annular dark field (HAADF) scanning electron microscopy for structural changes in thermally aged Ceria-Zirconia mixed oxides is investigated. The combined application of HRTEM and HAADF technique has allowed to interpret the superstructure contrasts observed in the HRTEM images of a cycled ceria-zirconia mixed oxide. It was found that the approach offers a powerful tool for characterizing structural rearrangements occurring in the cationic sublattice of these materials. It was also found that the approach allows to detect these structural effects at a nanoscale and earlier stages than those required by macroscopic techniques.},
address = {Departamento de Ciencia de los Maienales e Ingenieria Metalurgica y Quimica Inorganica, Facultad de Ciencias, Campus Puerto Real, 11510 C\'{a}diz, Spain},
annote = {Cited By (since 1996): 20
Export Date: 15 January 2013
Source: Scopus
CODEN: CMATE
doi: 10.1021/cm050976g
Language of Original Document: English
Correspondence Address: Calvino, J.J.; Departamento de Ciencia de los Maienales e Ingenieria Metalurgica y Quimica Inorganica, Facultad de Ciencias, Campus Puerto Real, 11510 C\'{a}diz, Spain; email: jose.calvino@uca.es
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author = {P\'{e}rez-Omil, JA. and Bernal, S. and Calvino, JJ. and Hern\'{a}ndez-Garrido, JC. and Mira, C. and Rodr\'{\i}guez-Luque, MP. and Erni, R. and Browning, ND.},
issn = {08974756 (ISSN)},
journal = {Chemistry of Materials},
keywords = {Age hardening,Ceria-Zirconia mixed oxides,Crystal lattices,Heat treatment,High resolution electron microscopy,High-angle annular dark field (HAADF) scanning ele,Positive ions,Scanning electron microscopy,Sublattices,Thermal ageign,Zirconia},
number = {17},
pages = {4282--4285},
title = {{Combined HREM and HAADF scanning transmission electron microscopy: A powerful tool for investigating structural changes in thermally aged Ceria-Zirconia mixed oxides}},
url = {https://www.scopus.com/inward/record.url?eid=2-s2.0-24944496885&partnerID=40&md5=b0a8ec860259046c6e39ce4a7f28040e},
volume = {17},
year = {2005}
}