@article{Perez-Omil2005,
abstract = {The technique of combined high-resolution transmission electron microscopy (HRTEM) and high-angle annular dark field (HAADF) scanning electron microscopy for structural changes in thermally aged Ceria-Zirconia mixed oxides is investigated. The combined application of HRTEM and HAADF technique has allowed to interpret the superstructure contrasts observed in the HRTEM images of a cycled ceria-zirconia mixed oxide. It was found that the approach offers a powerful tool for characterizing structural rearrangements occurring in the cationic sublattice of these materials. It was also found that the approach allows to detect these structural effects at a nanoscale and earlier stages than those required by macroscopic techniques.},
address = {Departamento de Ciencia de los Maienales e Ingenieria Metalurgica y Quimica Inorganica, Facultad de Ciencias, Campus Puerto Real, 11510 C{\'{a}}diz, Spain},
annote = {Cited By (since 1996): 20

        
Export Date: 15 January 2013

        
Source: Scopus

        
CODEN: CMATE

        
doi: 10.1021/cm050976g

        
Language of Original Document: English

        
Correspondence Address: Calvino, J.J.; Departamento de Ciencia de los Maienales e Ingenieria Metalurgica y Quimica Inorganica, Facultad de Ciencias, Campus Puerto Real, 11510 C{\'{a}}diz, Spain; email: jose.calvino@uca.es

        
References: Shelef, M., Graham, G.W., McCabe, R.W., (2002) Catalysis by Ceria and Related Materials, pp. 343-375. , Trovarelli, A., Ed.; Imperial College Press: London; Chapter 10; 
Izu, N., Omata, T., Otsuka-Yao-Matsuo, S., (1998) J. Alloys Compd., 270, p. 107; 
Baker, R.T., Bernal, S., Blanco, G., Cordon, A.M., Pintado, J.M., Rodr{\'{i}}guez-Izquierdo, J.M., Fally, F., Perrichon, V., (1999) Chem. Commun., p. 149; 
Fornasiero, P., Moniti, T., Graziani, M., Kaspar, J., Hungria, A.B., Mart{\'{i}}nez-Arias, A., Conesa, J.C., (2002) Phys. Chem. Chem. Phys., 4, p. 149; 
Montini, T., Ba{\~{n}}ares, M.A., Hickey, N., Di Monte, R., Fornasiero, P., Kaspar, J., Graziani, M., (2004) Phys. Chem. Chem. Phys., 6, p. 1; 
Montini, T., Hickey, N., Fornasiero, P., Graziani, M., Ba{\~{n}}ares, M.A., Mart{\'{i}}nez-Huerta, M.V., Alessandri, I., Depero, L.E., (2005) Chem. Mater., 17, p. 1157; 
Kishimoto, H., Omata, T., Otsuka-Yao-Matsuo, S., Ueda, K., Hosono, H., Kawazoe, H., (2000) J. Alloys Compd., 312, p. 94; 
Bernal, S., Botana, F.J., Calvino, J.J., L{\'{o}}pez Cartes, C., P{\'{e}}rez-Omil, J.A., Rodr{\'{i}}guez-Izquierdo, J.M., (1998) Ultramicroscopy, 72, p. 135; 
Stadelmann, P., (1987) Ultramicroscopy, 21, p. 131; 
Kirkland, E.J., (1998) Advanced Computing in Electron Microscopy, , Plenum Press: New York; 
Col{\'{o}}n, G., Pijolat, M., Valdivieso, F., Vidal, H., Kaspar, J., Fonochio, E., Daturi, M., Bernal, S., (1998) J. Chem. Soc., Faraday Trans., 94, p. 3717; 
Vidal, H., Bernal, S., Kaspar, J., Pijolat, M., Perrichon, V., Blanco, G., Pintado, J.M., Fally, F., (1999) Catal. Today, 54, p. 93; 
Torng, S., Miyazawa, K., Suzuki, K., Sakuma, T., (1994) Philos. Mag. A, 70, p. 505; 
Masui, T., Ozaki, T., Adachi, G., Kang, Z., Eyring, L., (2000) Chem. Lett., 7, p. 240; 
Pennycook, S.J., Boatner, A., (1988) Nature, 336, p. 565; 
Browning, N.D., Arslan, I., Moeck, P., Topuria, T., (2001) Phys. Status Solidi b, 227, p. 229; 
Zhao, H., Guillet, N., Valdivieso, F., Pijolat, M., (2003) Solid State Ionics, 160, p. 317; 
Mamontov, E., Brezny, R., Koranne, M., Egami, T., (2003) J. Phys. Chem. B, 107, p. 13007},
author = {P{\'{e}}rez-Omil, JA. and Bernal, S. and Calvino, JJ. and Hern{\'{a}}ndez-Garrido, JC. and Mira, C. and Rodr{\'{i}}guez-Luque, MP. and Erni, R. and Browning, ND.},
issn = {08974756 (ISSN)},
journal = {Chemistry of Materials},
keywords = {Age hardening,Ceria-Zirconia mixed oxides,Crystal lattices,Heat treatment,High resolution electron microscopy,High-angle annular dark field (HAADF) scanning ele,Positive ions,Scanning electron microscopy,Sublattices,Thermal ageign,Zirconia},
number = {17},
pages = {4282--4285},
title = {{Combined HREM and HAADF scanning transmission electron microscopy: A powerful tool for investigating structural changes in thermally aged Ceria-Zirconia mixed oxides}},
url = {https://www.scopus.com/inward/record.url?eid=2-s2.0-24944496885{\&}partnerID=40{\&}md5=b0a8ec860259046c6e39ce4a7f28040e},
volume = {17},
year = {2005}
}

{"_id":"mu4HqgEaXiL3xM5e5","bibbaseid":"prezomil-bernal-calvino-hernndezgarrido-mira-rodriguezluque-erni-browning-combinedhremandhaadfscanningtransmissionelectronmicroscopyapowerfultoolforinvestigatingstructuralchangesinthermallyagedceriazirconiamixedoxides-2005","downloads":0,"creationDate":"2016-04-21T11:02:49.512Z","title":"Combined HREM and HAADF scanning transmission electron microscopy: A powerful tool for investigating structural changes in thermally aged Ceria-Zirconia mixed oxides","author_short":["Pérez-Omil, J.","Bernal, S.","Calvino, J.","Hernández-Garrido, J.","Mira, C.","Rodríguez-Luque, M.","Erni, R.","Browning, N."],"year":2005,"bibtype":"article","biburl":"www2.uca.es/dept/cmat_qinor/nanomat/people/Hernandez.bib","bibdata":{"bibtype":"article","type":"article","abstract":"The technique of combined high-resolution transmission electron microscopy (HRTEM) and high-angle annular dark field (HAADF) scanning electron microscopy for structural changes in thermally aged Ceria-Zirconia mixed oxides is investigated. The combined application of HRTEM and HAADF technique has allowed to interpret the superstructure contrasts observed in the HRTEM images of a cycled ceria-zirconia mixed oxide. It was found that the approach offers a powerful tool for characterizing structural rearrangements occurring in the cationic sublattice of these materials. It was also found that the approach allows to detect these structural effects at a nanoscale and earlier stages than those required by macroscopic techniques.","address":"Departamento de Ciencia de los Maienales e Ingenieria Metalurgica y Quimica Inorganica, Facultad de Ciencias, Campus Puerto Real, 11510 Cádiz, Spain","annote":"Cited By (since 1996): 20 Export Date: 15 January 2013 Source: Scopus CODEN: CMATE doi: 10.1021/cm050976g Language of Original Document: English Correspondence Address: Calvino, J.J.; Departamento de Ciencia de los Maienales e Ingenieria Metalurgica y Quimica Inorganica, Facultad de Ciencias, Campus Puerto Real, 11510 Cádiz, Spain; email: jose.calvino@uca.es References: Shelef, M., Graham, G.W., McCabe, R.W., (2002) Catalysis by Ceria and Related Materials, pp. 343-375. , Trovarelli, A., Ed.; Imperial College Press: London; Chapter 10; Izu, N., Omata, T., Otsuka-Yao-Matsuo, S., (1998) J. Alloys Compd., 270, p. 107; Baker, R.T., Bernal, S., Blanco, G., Cordon, A.M., Pintado, J.M., Rodríguez-Izquierdo, J.M., Fally, F., Perrichon, V., (1999) Chem. Commun., p. 149; Fornasiero, P., Moniti, T., Graziani, M., Kaspar, J., Hungria, A.B., Martínez-Arias, A., Conesa, J.C., (2002) Phys. Chem. Chem. Phys., 4, p. 149; Montini, T., Bañares, M.A., Hickey, N., Di Monte, R., Fornasiero, P., Kaspar, J., Graziani, M., (2004) Phys. Chem. Chem. Phys., 6, p. 1; Montini, T., Hickey, N., Fornasiero, P., Graziani, M., Bañares, M.A., Martínez-Huerta, M.V., Alessandri, I., Depero, L.E., (2005) Chem. Mater., 17, p. 1157; Kishimoto, H., Omata, T., Otsuka-Yao-Matsuo, S., Ueda, K., Hosono, H., Kawazoe, H., (2000) J. Alloys Compd., 312, p. 94; Bernal, S., Botana, F.J., Calvino, J.J., López Cartes, C., Pérez-Omil, J.A., Rodríguez-Izquierdo, J.M., (1998) Ultramicroscopy, 72, p. 135; Stadelmann, P., (1987) Ultramicroscopy, 21, p. 131; Kirkland, E.J., (1998) Advanced Computing in Electron Microscopy, , Plenum Press: New York; Colón, G., Pijolat, M., Valdivieso, F., Vidal, H., Kaspar, J., Fonochio, E., Daturi, M., Bernal, S., (1998) J. Chem. Soc., Faraday Trans., 94, p. 3717; Vidal, H., Bernal, S., Kaspar, J., Pijolat, M., Perrichon, V., Blanco, G., Pintado, J.M., Fally, F., (1999) Catal. Today, 54, p. 93; Torng, S., Miyazawa, K., Suzuki, K., Sakuma, T., (1994) Philos. Mag. A, 70, p. 505; Masui, T., Ozaki, T., Adachi, G., Kang, Z., Eyring, L., (2000) Chem. Lett., 7, p. 240; Pennycook, S.J., Boatner, A., (1988) Nature, 336, p. 565; Browning, N.D., Arslan, I., Moeck, P., Topuria, T., (2001) Phys. Status Solidi b, 227, p. 229; Zhao, H., Guillet, N., Valdivieso, F., Pijolat, M., (2003) Solid State Ionics, 160, p. 317; Mamontov, E., Brezny, R., Koranne, M., Egami, T., (2003) J. Phys. Chem. 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The combined application of HRTEM and HAADF technique has allowed to interpret the superstructure contrasts observed in the HRTEM images of a cycled ceria-zirconia mixed oxide. It was found that the approach offers a powerful tool for characterizing structural rearrangements occurring in the cationic sublattice of these materials. It was also found that the approach allows to detect these structural effects at a nanoscale and earlier stages than those required by macroscopic techniques.},\r\naddress = {Departamento de Ciencia de los Maienales e Ingenieria Metalurgica y Quimica Inorganica, Facultad de Ciencias, Campus Puerto Real, 11510 C{\\'{a}}diz, Spain},\r\nannote = {Cited By (since 1996): 20\r\n\r\n \r\nExport Date: 15 January 2013\r\n\r\n \r\nSource: Scopus\r\n\r\n \r\nCODEN: CMATE\r\n\r\n \r\ndoi: 10.1021/cm050976g\r\n\r\n \r\nLanguage of Original Document: English\r\n\r\n \r\nCorrespondence Address: Calvino, J.J.; Departamento de Ciencia de los Maienales e Ingenieria Metalurgica y Quimica Inorganica, Facultad de Ciencias, Campus Puerto Real, 11510 C{\\'{a}}diz, Spain; email: jose.calvino@uca.es\r\n\r\n \r\nReferences: Shelef, M., Graham, G.W., McCabe, R.W., (2002) Catalysis by Ceria and Related Materials, pp. 343-375. , Trovarelli, A., Ed.; Imperial College Press: London; Chapter 10; \r\nIzu, N., Omata, T., Otsuka-Yao-Matsuo, S., (1998) J. Alloys Compd., 270, p. 107; \r\nBaker, R.T., Bernal, S., Blanco, G., Cordon, A.M., Pintado, J.M., Rodr{\\'{i}}guez-Izquierdo, J.M., Fally, F., Perrichon, V., (1999) Chem. Commun., p. 149; \r\nFornasiero, P., Moniti, T., Graziani, M., Kaspar, J., Hungria, A.B., Mart{\\'{i}}nez-Arias, A., Conesa, J.C., (2002) Phys. Chem. Chem. Phys., 4, p. 149; \r\nMontini, T., Ba{\\~{n}}ares, M.A., Hickey, N., Di Monte, R., Fornasiero, P., Kaspar, J., Graziani, M., (2004) Phys. Chem. Chem. Phys., 6, p. 1; \r\nMontini, T., Hickey, N., Fornasiero, P., Graziani, M., Ba{\\~{n}}ares, M.A., Mart{\\'{i}}nez-Huerta, M.V., Alessandri, I., Depero, L.E., (2005) Chem. Mater., 17, p. 1157; \r\nKishimoto, H., Omata, T., Otsuka-Yao-Matsuo, S., Ueda, K., Hosono, H., Kawazoe, H., (2000) J. Alloys Compd., 312, p. 94; \r\nBernal, S., Botana, F.J., Calvino, J.J., L{\\'{o}}pez Cartes, C., P{\\'{e}}rez-Omil, J.A., Rodr{\\'{i}}guez-Izquierdo, J.M., (1998) Ultramicroscopy, 72, p. 135; \r\nStadelmann, P., (1987) Ultramicroscopy, 21, p. 131; \r\nKirkland, E.J., (1998) Advanced Computing in Electron Microscopy, , Plenum Press: New York; \r\nCol{\\'{o}}n, G., Pijolat, M., Valdivieso, F., Vidal, H., Kaspar, J., Fonochio, E., Daturi, M., Bernal, S., (1998) J. Chem. Soc., Faraday Trans., 94, p. 3717; \r\nVidal, H., Bernal, S., Kaspar, J., Pijolat, M., Perrichon, V., Blanco, G., Pintado, J.M., Fally, F., (1999) Catal. Today, 54, p. 93; \r\nTorng, S., Miyazawa, K., Suzuki, K., Sakuma, T., (1994) Philos. Mag. A, 70, p. 505; \r\nMasui, T., Ozaki, T., Adachi, G., Kang, Z., Eyring, L., (2000) Chem. Lett., 7, p. 240; \r\nPennycook, S.J., Boatner, A., (1988) Nature, 336, p. 565; \r\nBrowning, N.D., Arslan, I., Moeck, P., Topuria, T., (2001) Phys. Status Solidi b, 227, p. 229; \r\nZhao, H., Guillet, N., Valdivieso, F., Pijolat, M., (2003) Solid State Ionics, 160, p. 317; \r\nMamontov, E., Brezny, R., Koranne, M., Egami, T., (2003) J. Phys. Chem. 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