Modification of glass ionomer cement by incorporating hydroxyapatite-silica nano-powder composite: Sol-gel synthesis and characterization. Shiekh, R. A., Ab Rahman, I., Masudi, S. M., & Luddin, N. Ceramics International, 40(2):3165–3170, March, 2014. WOS:000329882100079
doi  abstract   bibtex   
A nanohydroxyapatite-silica powder was synthesized using an ethanol based sol-gel technique. The synthesized powder was incorporated into commercial glass ionomer powder (Fuji II GC) and characterized using FTIR, Si-29 CP/MAS NMR, EDX and XRD spectroscopy. Si-29 CP/MAS NMR results showed the presence of higher degree of cross-linking of silyl species between silica and GIC, which makes the Nano-HA-Silica-GIC composite much stronger. High-resolution transmission electron microscopy (TEM) and scanning electron microscopy (TEM) was employed to investigate the morphology of the synthesized powder. Results revealed that higher content of nanosilica produced a denser and stronger GIC. Thus, the application of nanohydroxyapatite-silica-GIC with improved properties are envisioned to be of great clinical importance, especially in stress bearing areas. (C) 2013 Elsevier Ltd and Techna Group S.r.l. All rights reserved.
@article{shiekh_modification_2014,
	title = {Modification of glass ionomer cement by incorporating hydroxyapatite-silica nano-powder composite: {Sol}-gel synthesis and characterization},
	volume = {40},
	issn = {0272-8842},
	shorttitle = {Modification of glass ionomer cement by incorporating hydroxyapatite-silica nano-powder composite},
	doi = {10.1016/j.ceramint.2013.09.127},
	abstract = {A nanohydroxyapatite-silica powder was synthesized using an ethanol based sol-gel technique. The synthesized powder was incorporated into commercial glass ionomer powder (Fuji II GC) and characterized using FTIR, Si-29 CP/MAS NMR, EDX and XRD spectroscopy. Si-29 CP/MAS NMR results showed the presence of higher degree of cross-linking of silyl species between silica and GIC, which makes the Nano-HA-Silica-GIC composite much stronger. High-resolution transmission electron microscopy (TEM) and scanning electron microscopy (TEM) was employed to investigate the morphology of the synthesized powder. Results revealed that higher content of nanosilica produced a denser and stronger GIC. Thus, the application of nanohydroxyapatite-silica-GIC with improved properties are envisioned to be of great clinical importance, especially in stress bearing areas. (C) 2013 Elsevier Ltd and Techna Group S.r.l. All rights reserved.},
	language = {English},
	number = {2},
	journal = {Ceramics International},
	author = {Shiekh, Rayees Ahmad and Ab Rahman, Ismail and Masudi, Sam'an Malik and Luddin, Norhayati},
	month = mar,
	year = {2014},
	note = {WOS:000329882100079},
	keywords = {Glass ionomer cement, Silica-nanohydroxyapatite, Sol-gel technique, characterization, dentistry, particles, phosphate, strength},
	pages = {3165--3170},
}

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