Modification of glass ionomer cement by incorporating hydroxyapatite-silica nano-powder composite: Sol-gel synthesis and characterization. Shiekh, R. A., Ab Rahman, I., Masudi, S. M., & Luddin, N. Ceramics International, 40(2):3165–3170, March, 2014. WOS:000329882100079doi abstract bibtex A nanohydroxyapatite-silica powder was synthesized using an ethanol based sol-gel technique. The synthesized powder was incorporated into commercial glass ionomer powder (Fuji II GC) and characterized using FTIR, Si-29 CP/MAS NMR, EDX and XRD spectroscopy. Si-29 CP/MAS NMR results showed the presence of higher degree of cross-linking of silyl species between silica and GIC, which makes the Nano-HA-Silica-GIC composite much stronger. High-resolution transmission electron microscopy (TEM) and scanning electron microscopy (TEM) was employed to investigate the morphology of the synthesized powder. Results revealed that higher content of nanosilica produced a denser and stronger GIC. Thus, the application of nanohydroxyapatite-silica-GIC with improved properties are envisioned to be of great clinical importance, especially in stress bearing areas. (C) 2013 Elsevier Ltd and Techna Group S.r.l. All rights reserved.
@article{shiekh_modification_2014,
title = {Modification of glass ionomer cement by incorporating hydroxyapatite-silica nano-powder composite: {Sol}-gel synthesis and characterization},
volume = {40},
issn = {0272-8842},
shorttitle = {Modification of glass ionomer cement by incorporating hydroxyapatite-silica nano-powder composite},
doi = {10.1016/j.ceramint.2013.09.127},
abstract = {A nanohydroxyapatite-silica powder was synthesized using an ethanol based sol-gel technique. The synthesized powder was incorporated into commercial glass ionomer powder (Fuji II GC) and characterized using FTIR, Si-29 CP/MAS NMR, EDX and XRD spectroscopy. Si-29 CP/MAS NMR results showed the presence of higher degree of cross-linking of silyl species between silica and GIC, which makes the Nano-HA-Silica-GIC composite much stronger. High-resolution transmission electron microscopy (TEM) and scanning electron microscopy (TEM) was employed to investigate the morphology of the synthesized powder. Results revealed that higher content of nanosilica produced a denser and stronger GIC. Thus, the application of nanohydroxyapatite-silica-GIC with improved properties are envisioned to be of great clinical importance, especially in stress bearing areas. (C) 2013 Elsevier Ltd and Techna Group S.r.l. All rights reserved.},
language = {English},
number = {2},
journal = {Ceramics International},
author = {Shiekh, Rayees Ahmad and Ab Rahman, Ismail and Masudi, Sam'an Malik and Luddin, Norhayati},
month = mar,
year = {2014},
note = {WOS:000329882100079},
keywords = {Glass ionomer cement, Silica-nanohydroxyapatite, Sol-gel technique, characterization, dentistry, particles, phosphate, strength},
pages = {3165--3170},
}
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Si-29 CP/MAS NMR results showed the presence of higher degree of cross-linking of silyl species between silica and GIC, which makes the Nano-HA-Silica-GIC composite much stronger. High-resolution transmission electron microscopy (TEM) and scanning electron microscopy (TEM) was employed to investigate the morphology of the synthesized powder. Results revealed that higher content of nanosilica produced a denser and stronger GIC. Thus, the application of nanohydroxyapatite-silica-GIC with improved properties are envisioned to be of great clinical importance, especially in stress bearing areas. (C) 2013 Elsevier Ltd and Techna Group S.r.l. All rights reserved.","language":"English","number":"2","journal":"Ceramics International","author":[{"propositions":[],"lastnames":["Shiekh"],"firstnames":["Rayees","Ahmad"],"suffixes":[]},{"propositions":[],"lastnames":["Ab","Rahman"],"firstnames":["Ismail"],"suffixes":[]},{"propositions":[],"lastnames":["Masudi"],"firstnames":["Sam'an","Malik"],"suffixes":[]},{"propositions":[],"lastnames":["Luddin"],"firstnames":["Norhayati"],"suffixes":[]}],"month":"March","year":"2014","note":"WOS:000329882100079","keywords":"Glass ionomer cement, Silica-nanohydroxyapatite, Sol-gel technique, characterization, dentistry, particles, phosphate, strength","pages":"3165–3170","bibtex":"@article{shiekh_modification_2014,\n\ttitle = {Modification of glass ionomer cement by incorporating hydroxyapatite-silica nano-powder composite: {Sol}-gel synthesis and characterization},\n\tvolume = {40},\n\tissn = {0272-8842},\n\tshorttitle = {Modification of glass ionomer cement by incorporating hydroxyapatite-silica nano-powder composite},\n\tdoi = {10.1016/j.ceramint.2013.09.127},\n\tabstract = {A nanohydroxyapatite-silica powder was synthesized using an ethanol based sol-gel technique. 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