Comprehensive Two-Dimensional Gas Chromatographic Analysis of Volatile Organic Compounds in Distillate of Fermented Sorbus Domestica Fruit. Vyviurska, O., Pysarevska, S., Jánošková, N., & Špánik, I.
Comprehensive Two-Dimensional Gas Chromatographic Analysis of Volatile Organic Compounds in Distillate of Fermented Sorbus Domestica Fruit [link]Paper  doi  abstract   bibtex   
The Slovak-Czech spirit distilled from Sorbus domestica was analyzed by GCxGC with headspace solid phase microextraction and liquid-liquid extraction. Two column combinations, nonpolar × medium-polar and polar × medium-polar were tested. The second column setup provided more exploited 2D separation space with better distribution of peaks in chromatogram. Effects of the first column on the elution order of γ-lactones, benzyl esters, and unsaturated aldehydes in the second separation were observed. More than 500 compounds were detected; nearly 100 were confirmed with standards.
@article{vyviurskaComprehensiveTwodimensionalGas2015,
  title = {Comprehensive Two-Dimensional Gas Chromatographic Analysis of Volatile Organic Compounds in Distillate of Fermented {{Sorbus}} Domestica Fruit},
  author = {Vyviurska, Olga and Pysarevska, Solomiya and Jánošková, Nikoleta and Špánik, Ivan},
  date = {2015-01},
  journaltitle = {Open Chemistry},
  volume = {13},
  issn = {2391-5420},
  doi = {10.1515/chem-2015-0007},
  url = {https://doi.org/10.1515/chem-2015-0007},
  abstract = {The Slovak-Czech spirit distilled from Sorbus domestica was analyzed by GCxGC with headspace solid phase microextraction and liquid-liquid extraction. Two column combinations, nonpolar × medium-polar and polar × medium-polar were tested. The second column setup provided more exploited 2D separation space with better distribution of peaks in chromatogram. Effects of the first column on the elution order of γ-lactones, benzyl esters, and unsaturated aldehydes in the second separation were observed. More than 500 compounds were detected; nearly 100 were confirmed with standards.},
  keywords = {*imported-from-citeulike-INRMM,~INRMM-MiD:c-13435050,alcoholic-beverage,sorbus-domestica,two-dimensional-gas-chromatography},
  number = {1}
}

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