First stage of thermal aging under oxidizing conditions of a Ce 0.62Zr0.38O2 mixed oxide with an ordered cationic sublattice: A chemical, nanostructural, and nanoanalytical study. Yeste, M., Hernández-Garrido, J., Trasobares, S., Bernal, S., Blanco, G., Calvino, J., Pérez-Omil, J., & Pintado, J. Chemistry of Materials, 20(15):5107–5113, Departamento de Ciencia de Los Materiales e Ingenieria Metalurgica y Quimica Inorganica, Facultad de Ciencias, Campus Rio San Pedro, Puerto Real, E-11510-Cádiz, Spain, 2008. Paper abstract bibtex After being heated in a flow of 5% O2/He, at 1073 or 1123 K for 30 min, a Ce0.62Zr0.38O2 sample showing an ordered cationic sublattice had very subtle surface nanostructural changes induced on it. In parallel with them, a significant loss of low-temperature (77 < 773 K) oxygen storage capacity (OSC), with no modification of its high-temperature (T > 973 K) redox response, was observed. These nanostructural and chemical features characterize the very first stage of the process leading to the destruction of the ordered Ce-Zr sublattice, a structural phenomenon playing a key role in the control of redox behavior of ceria-zirconia mixed oxides. The reported results, including OSC, hydrogen chemisorption, and nanostructural and nanoanalytical data, lend further support to a model providing a comprehensive interpretation of the complex relationship linking thermal aging conditions, nanostructural properties, surface chemistry, and redox behavior in these materials. © 2008 American Chemical Society.
@article{Yeste2008,
abstract = {After being heated in a flow of 5% O2/He, at 1073 or 1123 K for 30 min, a Ce0.62Zr0.38O2 sample showing an ordered cationic sublattice had very subtle surface nanostructural changes induced on it. In parallel with them, a significant loss of low-temperature (77 < 773 K) oxygen storage capacity (OSC), with no modification of its high-temperature (T > 973 K) redox response, was observed. These nanostructural and chemical features characterize the very first stage of the process leading to the destruction of the ordered Ce-Zr sublattice, a structural phenomenon playing a key role in the control of redox behavior of ceria-zirconia mixed oxides. The reported results, including OSC, hydrogen chemisorption, and nanostructural and nanoanalytical data, lend further support to a model providing a comprehensive interpretation of the complex relationship linking thermal aging conditions, nanostructural properties, surface chemistry, and redox behavior in these materials. © 2008 American Chemical Society.},
address = {Departamento de Ciencia de Los Materiales e Ingenieria Metalurgica y Quimica Inorganica, Facultad de Ciencias, Campus Rio San Pedro, Puerto Real, E-11510-C\'{a}diz, Spain},
annote = {Cited By (since 1996): 18
Export Date: 15 January 2013
Source: Scopus
CODEN: CMATE
doi: 10.1021/cm800928p
Language of Original Document: English
Correspondence Address: Bernal, S.; Departamento de Ciencia de Los Materiales e Ingenieria Metalurgica y Quimica Inorganica, Facultad de Ciencias, Campus Rio San Pedro, Puerto Real, E-11510-C\'{a}diz, Spain; email: serafin.bernal@uca.es
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Lemaux, S., Bensaddik, A., van der Eerden, A.M.J., Bitter, J.H., Koningsberger, D.C., (2001) J. Phys. Chem. B, 105, p. 4810},
author = {Yeste, MP. and Hern\'{a}ndez-Garrido, JC. and Trasobares, S. and Bernal, S. and Blanco, G. and Calvino, JJ. and P\'{e}rez-Omil, JA. and Pintado, JM.},
issn = {08974756 (ISSN)},
journal = {Chemistry of Materials},
keywords = {Cerium,Cerium compounds,Oxidizing conditions,Thermal aging},
number = {15},
pages = {5107--5113},
title = {{First stage of thermal aging under oxidizing conditions of a Ce 0.62Zr0.38O2 mixed oxide with an ordered cationic sublattice: A chemical, nanostructural, and nanoanalytical study}},
url = {https://www.scopus.com/inward/record.url?eid=2-s2.0-50249129711&partnerID=40&md5=b8ce291c2878bc5f863b6cce81f28826},
volume = {20},
year = {2008}
}
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In parallel with them, a significant loss of low-temperature (77 < 773 K) oxygen storage capacity (OSC), with no modification of its high-temperature (T > 973 K) redox response, was observed. These nanostructural and chemical features characterize the very first stage of the process leading to the destruction of the ordered Ce-Zr sublattice, a structural phenomenon playing a key role in the control of redox behavior of ceria-zirconia mixed oxides. The reported results, including OSC, hydrogen chemisorption, and nanostructural and nanoanalytical data, lend further support to a model providing a comprehensive interpretation of the complex relationship linking thermal aging conditions, nanostructural properties, surface chemistry, and redox behavior in these materials. © 2008 American Chemical Society.","address":"Departamento de Ciencia de Los Materiales e Ingenieria Metalurgica y Quimica Inorganica, Facultad de Ciencias, Campus Rio San Pedro, Puerto Real, E-11510-Cádiz, Spain","annote":"Cited By (since 1996): 18 Export Date: 15 January 2013 Source: Scopus CODEN: CMATE doi: 10.1021/cm800928p Language of Original Document: English Correspondence Address: Bernal, S.; Departamento de Ciencia de Los Materiales e Ingenieria Metalurgica y Quimica Inorganica, Facultad de Ciencias, Campus Rio San Pedro, Puerto Real, E-11510-Cádiz, Spain; email: serafin.bernal@uca.es References: Izu, N., Omata, T., Otsuka-Yao-Matsuo, S., (1998) J. Alloys Compd, 270, p. 107; Otsuka-Yao-Matsuo, S., Omata, T., Izu, N., Kishimoto, H., (1998) J. Solid State Chem, 138, p. 47; Baker, R.T., Bernai, S., Blanco, G., Cordón, A.M., Pintado, J.M., Rodríguez-Izquierdo, J.M., Fally, F., Perrichon, V., (1999) Chem. Commun. (Cambridge, U.K.), p. 149; Fornasiero, P., Montini, T., Graziani, M., Kaspar, J., Hungría, A.B., Martínez-Arias, A., Conesa, J.C., (2002) Phys. Chem. Chem. Phys, 4, p. 149; Suda, A., Ukyo, Y., Yamamura, K., Sobukawa, H., Sasaki, T., Nagai, Y., Tanabe, T., Sugiura, M.J., (2004) Ceram. Soc. Jpn, 172, p. 586; Montini, T., Hickey, N., Fornasiero, P., Graziani, M., Bañares, M.A., Martínez-Huerta, M.V., Alessandri, I., Depero, L.E., (2005) Chem. Mater, 17, p. 1157; Alessandri, I., Bañares, M.A., Depero, L.E., Ferroni, M., Fornasiero, P., Gennari, F.C., Hickey, N., Montini, T., (2006) Top. Catal, 41, p. 35; Zhao, M., Shen, M., Wang, J., (2007) J. Catal, 248, p. 258; Mamontov, E., Brezny, R., Koranne, M., Egami, T., (2003) J. Phys. Chem. B, 107, p. 13007; Mamontov, E., Egami, T., Brezny, R., Koranne, M., Tyagi, S., (2000) J. Phys. Chem. B, 104, p. 11110; Wang, R., Crozier, P.A., Sharma, R., Adams, J.B., (2006) J. Phys. Chem. B, 170, p. 18278; Putna, E.S., Bunluesin, T., Fan, X.L., Gorte, R.J., Vohs, J.M., Lakis, R.E., Egami, T., (1999) Catal. Today, 50, p. 343; Costa-Nunes, O., Gorte, R.G., Vohs, J.M., (2005) J. Mater. Chem, 15, p. 1520; Costa-Nunes, O., Ferrizz, R.M., Gorte, R.J., Vohs, J.M., (2005) Surf. Sci, 592, p. 8; Montini, T., Bañares, M.A., Hickey, N., Di Monte, R., Fornasiero, P., Kaspar, J., Graziani, M., (2004) Phys. Chem. Chem. Phys, 6, p. 1; Pérez Omil, J.A., Bernai, S., Calvino, J.J., Hernández, J.C., Mira, C., Rodríguez-Luque, M.P., Erni, R., Browning, N.D., (2005) Chem. Mater, 17, p. 4282; Sasaki, T., Ukyo, Y., Kuroda, K., Arai, S., Saka, H., (2003) J. Electron Microsc, 52, p. 309; Sasaki, T., Ukyo, Y., Suda, A., Sugiura, M., Kuroda, K., Arai, S., Saka, H.J., (2003) Ceram. Soc. Jpn, 111, p. 382; Izu, N., Kishimoto, H., Omata, T., Yao, T., Otsuka-Yao-Matsuo, S., (2001) Sci. Technol. Adv. Mater, 2, p. 443; Yeste, M.P., Hernández, J.C., Bernai, S., Blanco, G., Calvino, J.J., Pérez-Omil, J.A., Pintado, J.M., (2006) Chem. Mater, 18, p. 2750; Izu, N., Kishimoto, H., Omata, T., Yao, T., Otsuka-Yao-Matsuo, S., (2001) Sci. Technol. Adv. Mater, 2, p. 397; Hernández, J.C., Hungría, A.B., Pérez-Omil, J.A., Trasobares, S., Bernai, S., Midgley, P.A., Alavi, A., Calvino, J.J., (2007) J. Phys. Chem. C, 111, p. 9001; Kishimoto, H., Omata, T., Otsuka-Yao-Matsuo, S., Ueda, K., Hosono, H., Kawazoe, H., (2000) J. Alloys Compd, 312, p. 94; Bernal, S., Blanco, G., Calvino, J.J., Hernández, J.C., Pérez-Omil, J.A., Pintado, J.M., Yeste, M.P., (2008) J. Alloys Compd, 451, p. 521; Duprez, D., Descorme, C., (2002) Catalysis by Ceria and Related Materials, pp. 243-280. , Trovarelli, A, Ed, Imperial College Press: London, Ch. 7, pp; Aneggi, E., Boaro, M., de Leitenburg, C., Dolcetti, G., Trovarelli, A., (2006) J. Alloys Compd, 408-412, p. 1096; Vidal, H., Kaspar, J., Pijolat, M., Colón, G., Bernal, S., Cordón, A., Perrichon, V., Fally, F., (2001) Appl. Catal., B, 30, p. 75; Vidal, H., Bernal, S., Kaspar, J., Pijolat, M., Perrichon, V., Blanco, G., Pintado, J.M., Fally, F., (1999) Catal. Today, 54, p. 93; Norman, A., Perrichon, V., Bensaddik, A., Lemaux, S., Bitter, H., Koningsberger, D., (2001) Top. Catal, 16-17, p. 363; Gennari, F.C., Montini, T., Hickey, N., Fornasiero, P., Graziani, M., (2006) Appl. Surf. Sci, 252, p. 8456; Gatica, J.M., Baker, R.T., Fornasiero, P., Bernal, S., Blanco, G., Kaspar, J., (2000) J. Phys. Chem. B, 104, p. 4667; Collins, S.E., José, M., Cíes, J.M., del Río, E., López-Haro, M., Trasobares, S., Calvino, J.J., Bernai, S., (2007) J. Phys. Chem. C, 111, p. 14371; Colón, G., Pijolat, M., Valdivieso, F., Vidal, H., Kaspar, J., Finocchio, E., Daturi, M., Bernal, S., (1998) J. Chem. Soc., Faraday Trans, 94, p. 3111; Colón, G., Valdivieso, F., Pijolat, M., Baker, R.T., Calvino, J.J., Bernai, S., (1999) Catal. Today, 50, p. 271; Shah, P.R., Kim, T., Zhou, G., Fornasiero, P., Gorte, R.J., (2006) Chem. Mater, 18, p. 5363; Zhou, G., Shah, P.R., Kim, T., Fornasiero, P., Gorte, R.J., (2007) Catal. Today, 123, p. 86; Nagai, Y., Yamamoto, T., Tanaka, T., Yoshida, S., Nonaka, T., Okamoto, T., Suda, A., Sugiura, M., (2002) Catal. Today, 74, p. 225; Si, R., Zhang, Y.-W., Wang, L.-M., Li, S.-J., Lin, B.-X., Chu, W.-S., Wu, Z.-Y., Yan, C.-H., (2007) J. Phys. Chem. C, 11, p. 787; Lemaux, S., Bensaddik, A., van der Eerden, A.M.J., Bitter, J.H., Koningsberger, D.C., (2001) J. Phys. Chem. B, 105, p. 4810","author":[{"propositions":[],"lastnames":["Yeste"],"firstnames":["MP."],"suffixes":[]},{"propositions":[],"lastnames":["Hernández-Garrido"],"firstnames":["JC."],"suffixes":[]},{"propositions":[],"lastnames":["Trasobares"],"firstnames":["S."],"suffixes":[]},{"propositions":[],"lastnames":["Bernal"],"firstnames":["S."],"suffixes":[]},{"propositions":[],"lastnames":["Blanco"],"firstnames":["G."],"suffixes":[]},{"propositions":[],"lastnames":["Calvino"],"firstnames":["JJ."],"suffixes":[]},{"propositions":[],"lastnames":["Pérez-Omil"],"firstnames":["JA."],"suffixes":[]},{"propositions":[],"lastnames":["Pintado"],"firstnames":["JM."],"suffixes":[]}],"issn":"08974756 (ISSN)","journal":"Chemistry of Materials","keywords":"Cerium,Cerium compounds,Oxidizing conditions,Thermal aging","number":"15","pages":"5107–5113","title":"First stage of thermal aging under oxidizing conditions of a Ce 0.62Zr0.38O2 mixed oxide with an ordered cationic sublattice: A chemical, nanostructural, and nanoanalytical study","url":"https://www.scopus.com/inward/record.url?eid=2-s2.0-50249129711&partnerID=40&md5=b8ce291c2878bc5f863b6cce81f28826","volume":"20","year":"2008","bibtex":"@article{Yeste2008,\nabstract = {After being heated in a flow of 5% O2/He, at 1073 or 1123 K for 30 min, a Ce0.62Zr0.38O2 sample showing an ordered cationic sublattice had very subtle surface nanostructural changes induced on it. In parallel with them, a significant loss of low-temperature (77 < 773 K) oxygen storage capacity (OSC), with no modification of its high-temperature (T > 973 K) redox response, was observed. These nanostructural and chemical features characterize the very first stage of the process leading to the destruction of the ordered Ce-Zr sublattice, a structural phenomenon playing a key role in the control of redox behavior of ceria-zirconia mixed oxides. The reported results, including OSC, hydrogen chemisorption, and nanostructural and nanoanalytical data, lend further support to a model providing a comprehensive interpretation of the complex relationship linking thermal aging conditions, nanostructural properties, surface chemistry, and redox behavior in these materials. © 2008 American Chemical Society.},\naddress = {Departamento de Ciencia de Los Materiales e Ingenieria Metalurgica y Quimica Inorganica, Facultad de Ciencias, Campus Rio San Pedro, Puerto Real, E-11510-C\\'{a}diz, Spain},\nannote = {Cited By (since 1996): 18\n\n \nExport Date: 15 January 2013\n\n \nSource: Scopus\n\n \nCODEN: CMATE\n\n \ndoi: 10.1021/cm800928p\n\n \nLanguage of Original Document: English\n\n \nCorrespondence Address: Bernal, S.; Departamento de Ciencia de Los Materiales e Ingenieria Metalurgica y Quimica Inorganica, Facultad de Ciencias, Campus Rio San Pedro, Puerto Real, E-11510-C\\'{a}diz, Spain; email: serafin.bernal@uca.es\n\n \nReferences: Izu, N., Omata, T., Otsuka-Yao-Matsuo, S., (1998) J. Alloys Compd, 270, p. 107; \nOtsuka-Yao-Matsuo, S., Omata, T., Izu, N., Kishimoto, H., (1998) J. Solid State Chem, 138, p. 47; \nBaker, R.T., Bernai, S., Blanco, G., Cord\\'{o}n, A.M., Pintado, J.M., Rodr\\'{\\i}guez-Izquierdo, J.M., Fally, F., Perrichon, V., (1999) Chem. Commun. (Cambridge, U.K.), p. 149; \nFornasiero, P., Montini, T., Graziani, M., Kaspar, J., Hungr\\'{\\i}a, A.B., Mart\\'{\\i}nez-Arias, A., Conesa, J.C., (2002) Phys. Chem. Chem. Phys, 4, p. 149; \nSuda, A., Ukyo, Y., Yamamura, K., Sobukawa, H., Sasaki, T., Nagai, Y., Tanabe, T., Sugiura, M.J., (2004) Ceram. Soc. Jpn, 172, p. 586; \nMontini, T., Hickey, N., Fornasiero, P., Graziani, M., Ba\\~{n}ares, M.A., Mart\\'{\\i}nez-Huerta, M.V., Alessandri, I., Depero, L.E., (2005) Chem. Mater, 17, p. 1157; \nAlessandri, I., Ba\\~{n}ares, M.A., Depero, L.E., Ferroni, M., Fornasiero, P., Gennari, F.C., Hickey, N., Montini, T., (2006) Top. Catal, 41, p. 35; \nZhao, M., Shen, M., Wang, J., (2007) J. Catal, 248, p. 258; \nMamontov, E., Brezny, R., Koranne, M., Egami, T., (2003) J. Phys. Chem. B, 107, p. 13007; \nMamontov, E., Egami, T., Brezny, R., Koranne, M., Tyagi, S., (2000) J. Phys. Chem. B, 104, p. 11110; \nWang, R., Crozier, P.A., Sharma, R., Adams, J.B., (2006) J. Phys. Chem. B, 170, p. 18278; \nPutna, E.S., Bunluesin, T., Fan, X.L., Gorte, R.J., Vohs, J.M., Lakis, R.E., Egami, T., (1999) Catal. Today, 50, p. 343; \nCosta-Nunes, O., Gorte, R.G., Vohs, J.M., (2005) J. Mater. Chem, 15, p. 1520; \nCosta-Nunes, O., Ferrizz, R.M., Gorte, R.J., Vohs, J.M., (2005) Surf. Sci, 592, p. 8; \nMontini, T., Ba\\~{n}ares, M.A., Hickey, N., Di Monte, R., Fornasiero, P., Kaspar, J., Graziani, M., (2004) Phys. Chem. Chem. Phys, 6, p. 1; \nP\\'{e}rez Omil, J.A., Bernai, S., Calvino, J.J., Hern\\'{a}ndez, J.C., Mira, C., Rodr\\'{\\i}guez-Luque, M.P., Erni, R., Browning, N.D., (2005) Chem. Mater, 17, p. 4282; \nSasaki, T., Ukyo, Y., Kuroda, K., Arai, S., Saka, H., (2003) J. 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B, 105, p. 4810},\nauthor = {Yeste, MP. and Hern\\'{a}ndez-Garrido, JC. and Trasobares, S. and Bernal, S. and Blanco, G. and Calvino, JJ. and P\\'{e}rez-Omil, JA. and Pintado, JM.},\nissn = {08974756 (ISSN)},\njournal = {Chemistry of Materials},\nkeywords = {Cerium,Cerium compounds,Oxidizing conditions,Thermal aging},\nnumber = {15},\npages = {5107--5113},\ntitle = {{First stage of thermal aging under oxidizing conditions of a Ce 0.62Zr0.38O2 mixed oxide with an ordered cationic sublattice: A chemical, nanostructural, and nanoanalytical study}},\nurl = {https://www.scopus.com/inward/record.url?eid=2-s2.0-50249129711&partnerID=40&md5=b8ce291c2878bc5f863b6cce81f28826},\nvolume = {20},\nyear = {2008}\n}\n","author_short":["Yeste, M.","Hernández-Garrido, J.","Trasobares, S.","Bernal, S.","Blanco, G.","Calvino, J.","Pérez-Omil, J.","Pintado, J."],"key":"Yeste2008","id":"Yeste2008","bibbaseid":"yeste-hernndezgarrido-trasobares-bernal-blanco-calvino-prezomil-pintado-firststageofthermalagingunderoxidizingconditionsoface062zr038o2mixedoxidewithanorderedcationicsublatticeachemicalnanostructuralandnanoanalyticalstudy-2008","role":"author","urls":{"Paper":"https://www.scopus.com/inward/record.url?eid=2-s2.0-50249129711&partnerID=40&md5=b8ce291c2878bc5f863b6cce81f28826"},"keyword":["Cerium","Cerium compounds","Oxidizing conditions","Thermal aging"],"downloads":0,"html":"","metadata":{"authorlinks":{"yeste, m":"https://bibbase.org/show?bib=www2.uca.es%2Fdept%2Fcmat_qinor%2Fnanomat%2Fpeople%2FYeste.bib&groupby=year"}}},"search_terms":["first","stage","thermal","aging","under","oxidizing","conditions","62zr0","38o2","mixed","oxide","ordered","cationic","sublattice","chemical","nanostructural","nanoanalytical","study","yeste","hernández-garrido","trasobares","bernal","blanco","calvino","pérez-omil","pintado"],"keywords":["cerium","cerium compounds","oxidizing conditions","thermal aging"],"authorIDs":["7YCsQ2xSsE3dHbm2M"],"dataSources":["Re6vfFqp6mCGKxW5p","RZxB3KYJRtfBtYS47","cHrAkoGTxSAsg76Se","AZrZbPtRyjbHNBS3W"]}