Procedures for preparation of sealed powder patterns and single crystal samples for X-ray diffraction methods in controlled atmosphere without dry box. Zikmund, M. & Valent, A. Chemické zvesti (Chemical Papers), 23(11–12):934–937, 1969. Paper abstract bibtex In the present paper device and procedures are described for preparation of flat powdered samples of air-sensitive substances in an inert atmosphere without the application of a dry box. The samples are to be submitted to measurements with X-ray diffractograph and with the Guinier method. Further a method for filling single crystals into capillary tubes of Lindemann glass for measurements with the Weissenberg method are reported.
@article{Zikmund_Valent_1969,
author = "Zikmund, M. and Valent, A.",
title = "{Procedures for preparation of sealed powder patterns and single crystal samples for X-ray diffraction methods in controlled atmosphere without dry box}",
journal = "Chemické zvesti (Chemical Papers)",
year = "1969",
volume = "23",
number = "11--12",
pages = "934--937",
url = {https://www.chempap.org/file_access.php?file=2311-12a934.pdf},
abstract = {In the present paper device and procedures are described for preparation of flat powdered samples of air-sensitive substances in an inert atmosphere without the application of a dry box. The samples are to be submitted to measurements with X-ray diffractograph and with the Guinier method. Further a method for filling single crystals into capillary tubes of Lindemann glass for measurements with the Weissenberg method are reported.},
}
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