@article{
 title = {Synthesis and crystal structure of a palladium(II) complex with the amino acid L-citrulline},
 type = {article},
 year = {2015},
 keywords = {amino acids,palladium complex,powder diffraction,x-ray},
 pages = {357-361},
 volume = {30},
 websites = {http://www.journals.cambridge.org/abstract_S0885715615000652},
 month = {12},
 day = {2},
 id = {a41ff4dd-75ff-3f9b-b673-132e01f48b89},
 created = {2017-04-06T15:17:13.868Z},
 file_attached = {false},
 profile_id = {6d4e9e22-09e3-3340-83ee-25b0de1090e1},
 group_id = {90e2c5d9-8e7e-3658-9751-f62154fc0a37},
 last_modified = {2017-12-29T00:54:59.216Z},
 read = {false},
 starred = {false},
 authored = {false},
 confirmed = {false},
 hidden = {false},
 private_publication = {false},
 abstract = {Synthesis and structural characterization of a novel palladium Pd(II) complex with the amino acid L-citrulline (Cit, C 6 H 13 N 3 O 3 ) are presented in this paper. Elemental analysis indicates a 1:2 metal/ligand molar composition for the complex, with the molecular formula PdC 12 H 24 N 6 O 6. The compound was also characterized by infrared (IR) spectroscopic measurements and the crystal structure has been solved by powder X-ray diffraction data with simulated annealing strategy in real space. The Pd(II) complex crystallizes in the triclinic system with space group P-1 and cell parameters a = 4.6493(4) Å, b = 5.222(4) Å, c = 18.040(2) Å, α = 77.41(6)°, β = 94.72(7),° and γ = 101.45(7)°. The crystal structure confirms the presence of Pd(II) ions in a nearly square planar environment and the molecular formula with deprotonated citrulline as proposed by analytical and spectroscopic data.},
 bibtype = {article},
 author = {Mascaliovas, Bruno Z and Bergamini, Fernando R.G. and Cuin, Alexandre and Corbi, Pedro P},
 doi = {10.1017/S0885715615000652},
 journal = {Powder Diffraction},
 number = {04}
}

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Elemental analysis indicates a 1:2 metal/ligand molar composition for the complex, with the molecular formula PdC 12 H 24 N 6 O 6. The compound was also characterized by infrared (IR) spectroscopic measurements and the crystal structure has been solved by powder X-ray diffraction data with simulated annealing strategy in real space. The Pd(II) complex crystallizes in the triclinic system with space group P-1 and cell parameters a = 4.6493(4) Å, b = 5.222(4) Å, c = 18.040(2) Å, α = 77.41(6)°, β = 94.72(7),° and γ = 101.45(7)°. The crystal structure confirms the presence of Pd(II) ions in a nearly square planar environment and the molecular formula with deprotonated citrulline as proposed by analytical and spectroscopic data.","bibtype":"article","author":"Mascaliovas, Bruno Z and Bergamini, Fernando R.G. and Cuin, Alexandre and Corbi, Pedro P","doi":"10.1017/S0885715615000652","journal":"Powder Diffraction","number":"04","bibtex":"@article{\n title = {Synthesis and crystal structure of a palladium(II) complex with the amino acid L-citrulline},\n type = {article},\n year = {2015},\n keywords = {amino acids,palladium complex,powder diffraction,x-ray},\n pages = {357-361},\n volume = {30},\n websites = {http://www.journals.cambridge.org/abstract_S0885715615000652},\n month = {12},\n day = {2},\n id = {a41ff4dd-75ff-3f9b-b673-132e01f48b89},\n created = {2017-04-06T15:17:13.868Z},\n file_attached = {false},\n profile_id = {6d4e9e22-09e3-3340-83ee-25b0de1090e1},\n group_id = {90e2c5d9-8e7e-3658-9751-f62154fc0a37},\n last_modified = {2017-12-29T00:54:59.216Z},\n read = {false},\n starred = {false},\n authored = {false},\n confirmed = {false},\n hidden = {false},\n private_publication = {false},\n abstract = {Synthesis and structural characterization of a novel palladium Pd(II) complex with the amino acid L-citrulline (Cit, C 6 H 13 N 3 O 3 ) are presented in this paper. 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