@article{
 title = {Synthesis and crystal structure of a palladium(II) complex with the amino acid L-citrulline},
 type = {article},
 year = {2015},
 keywords = {[amino acids,palladium complex,powder diffractio},
 pages = {357-361},
 volume = {30},
 websites = {http://www.journals.cambridge.org/abstract_S0885715615000652},
 id = {d0bb8e3e-5d60-369c-a705-54cc926c9555},
 created = {2018-07-28T23:28:38.354Z},
 file_attached = {false},
 profile_id = {6d4e9e22-09e3-3340-83ee-25b0de1090e1},
 group_id = {edb17a89-a16c-3c5d-8f2a-ce318aa08fb4},
 last_modified = {2018-07-28T23:28:38.354Z},
 read = {false},
 starred = {false},
 authored = {false},
 confirmed = {true},
 hidden = {false},
 citation_key = {Mascaliovas2015},
 source_type = {article},
 private_publication = {false},
 abstract = {Synthesis and structural characterization of a novel palladium Pd(II) complex with the amino acid L-citrulline (Cit, C 6 H 13 N 3 O 3 ) are presented in this paper. Elemental analysis indicates a 1:2 metal/ligand molar composition for the complex, with the molecular formula PdC 12 H 24 N 6 O 6. The compound was also characterized by infrared (IR) spectroscopic measurements and the crystal structure has been solved by powder X-ray diffraction data with simulated annealing strategy in real space. The Pd(II) complex crystallizes in the triclinic system with space group P-1 and cell parameters a = 4.6493(4) Å, b = 5.222(4) Å, c = 18.040(2) Å, $α$ = 77.41(6)°, $β$ = 94.72(7),° and $γ$ = 101.45(7)°. The crystal structure confirms the presence of Pd(II) ions in a nearly square planar environment and the molecular formula with deprotonated citrulline as proposed by analytical and spectroscopic data.},
 bibtype = {article},
 author = {Mascaliovas, Bruno Z and Bergamini, Fernando R G and Cuin, Alexandre and Corbi, Pedro P},
 doi = {10.1017/S0885715615000652},
 journal = {Powder Diffraction},
 number = {04}
}

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Elemental analysis indicates a 1:2 metal/ligand molar composition for the complex, with the molecular formula PdC 12 H 24 N 6 O 6. The compound was also characterized by infrared (IR) spectroscopic measurements and the crystal structure has been solved by powder X-ray diffraction data with simulated annealing strategy in real space. The Pd(II) complex crystallizes in the triclinic system with space group P-1 and cell parameters a = 4.6493(4) Å, b = 5.222(4) Å, c = 18.040(2) Å, $α$ = 77.41(6)°, $β$ = 94.72(7),° and $γ$ = 101.45(7)°. 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